1-bromo-7-(2,3-dimethoxyphenyl)heptane

Base Information

Chemical Name:1-bromo-7-(2,3-dimethoxyphenyl)heptane
CAS No.:76014-93-2
Molecular Formula:C₁₅H₂₃BrO₂
Molecular Weight:315.25
Hs Code.:

Synonyms:1-bromo-7-(2,3-dimethoxyphenyl)heptane

Suppliers and Price of 1-bromo-7-(2,3-dimethoxyphenyl)heptane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-bromo-7-(2,3-dimethoxyphenyl)heptane

Chemical Property:

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Technology Process of 1-bromo-7-(2,3-dimethoxyphenyl)heptane

There total 10 articles about 1-bromo-7-(2,3-dimethoxyphenyl)heptane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 22.0%

: 91-16-7
1,2-dimethoxybenzene

: 4549-31-9
1,7-dibromoheptane

: 76014-93-2
1-bromo-7-(2,3-dimethoxyphenyl)heptane

Guidance literature:: With n-butyllithium; In tetrahydrofuran; hexane; for 4h; Heating;
DOI:10.1039/P19800002331

Reference yield:

: 53545-41-8
7-(2,3-dimethoxyphenyl)heptan-1-ol

: 76014-93-2
1-bromo-7-(2,3-dimethoxyphenyl)heptane

Guidance literature:: at 140 - 150 ℃; Einleiten von HBr und Behandeln des Reaktionsprodukts mit Dimethylsulfat und wss.-methanol. KOH;
DOI:10.1021/jo01189a012

Reference yield:

: 86-51-1
2,3-dimethyoxybenzaldehyde

: 76014-93-2
1-bromo-7-(2,3-dimethoxyphenyl)heptane

Guidance literature:: Multi-step reaction with 4 steps

1: Li / tetrahydrofuran / 16 h / -20 °C

2: aq. HCl / ethanol / 5 h / 35 - 40 °C

3: 45 percent / H₂; aq. HCl / 10 percent Pd/C / ethanol / 775.72 Torr

4: PBr₃ / CHCl₃ / 4 h / 20 °C

With hydrogenchloride; hydrogen; phosphorus tribromide; lithium; palladium on activated charcoal; In tetrahydrofuran; ethanol; chloroform;
DOI:10.1016/S0009-3084(02)00125-1