Technology Process of 3-(pentadec-8-ynyl)veratrole
There total 14 articles about 3-(pentadec-8-ynyl)veratrole which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
n-butyllithium;
In
tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; hexane;
for 24h;
Ambient temperature;
DOI:10.1039/P19800002331
- Guidance literature:
-
Multi-step reaction with 5 steps
1: Li / tetrahydrofuran / 16 h / -20 °C
2: aq. HCl / ethanol / 5 h / 35 - 40 °C
3: 45 percent / H2; aq. HCl / 10 percent Pd/C / ethanol / 775.72 Torr
4: PBr3 / CHCl3 / 4 h / 20 °C
5: HMPT / tetrahydrofuran / -50 °C
With
hydrogenchloride; N,N,N,N,N,N-hexamethylphosphoric triamide; hydrogen; phosphorus tribromide; lithium;
palladium on activated charcoal;
In
tetrahydrofuran; ethanol; chloroform;
DOI:10.1016/S0009-3084(02)00125-1
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 88 percent / p-TsOH / 1 h
2: Li / tetrahydrofuran / 16 h / -20 °C
3: aq. HCl / ethanol / 5 h / 35 - 40 °C
4: 45 percent / H2; aq. HCl / 10 percent Pd/C / ethanol / 775.72 Torr
5: PBr3 / CHCl3 / 4 h / 20 °C
6: HMPT / tetrahydrofuran / -50 °C
With
hydrogenchloride; N,N,N,N,N,N-hexamethylphosphoric triamide; hydrogen; phosphorus tribromide; lithium; toluene-4-sulfonic acid;
palladium on activated charcoal;
In
tetrahydrofuran; ethanol; chloroform;
DOI:10.1016/S0009-3084(02)00125-1
