{bis(η-cyclopentadienyl)(μ-carbonyl)(μ-bis(diphenylphosphinomethane))dirhodium}

Base Information

Chemical Name:{bis(η-cyclopentadienyl)(μ-carbonyl)(μ-bis(diphenylphosphinomethane))dirhodium}
CAS No.:88979-33-3
Molecular Formula:C₃₆H₃₂OP₂Rh₂
Molecular Weight:748.408
Hs Code.:

Synonyms:{bis(η-cyclopentadienyl)(μ-carbonyl)(μ-bis(diphenylphosphinomethane))dirhodium}

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Chemical Property of {bis(η-cyclopentadienyl)(μ-carbonyl)(μ-bis(diphenylphosphinomethane))dirhodium}

Chemical Property:

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Technology Process of {bis(η-cyclopentadienyl)(μ-carbonyl)(μ-bis(diphenylphosphinomethane))dirhodium}

There total 3 articles about {bis(η-cyclopentadienyl)(μ-carbonyl)(μ-bis(diphenylphosphinomethane))dirhodium} which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: dicyclopentadienyltricarbonyldirhodium

: 2071-20-7
bis-diphenylphosphinomethane

: 88979-33-3
{bis(η-cyclopentadienyl)(μ-carbonyl)(μ-bis(diphenylphosphinomethane))dirhodium}

Guidance literature:: In diethyl ether; to Et2O soln. of Rh-complex in Et2O was added dppm in Et2O with stirring under N2 for 1 h; filtered, washed with pentane, dried; elem. anal.;
DOI:10.1039/DT9840000533

Reference yield:

: 110682-61-6
bis(η-cyclopentadienyl)(μ-carbonyl)(μ-bis(diphenylphosphino)methane)(μ-copperchloride)dirhodium

: 88979-33-3
{bis(η-cyclopentadienyl)(μ-carbonyl)(μ-bis(diphenylphosphinomethane))dirhodium}

: 47107-74-4
tetrameric (triphenylphosphine)copper(I) iodide

Guidance literature:: With triphenyl phosphine; In dichloromethane; a stoich. amount of PPh3 was added to a CH2Cl2 soln. of Rh2Cu-cluster under N2, mixt. was stirred for ca. 30 min at room temp.; evapd., residue was extd. with Et2O, Rh2-complex was isolated from the ext., solid residue was characterized as Cu(PPh3)I by comparison with autentic sample;

Reference yield:

: 110682-60-5
{bis(η-cyclopentadienyl)(μ-carbonyl)(μ-bis(diphenylphosphino)methane)(μ-copperchloride)}dirhodium

: 22176-30-3
(triphenylphosphine)CuCl

: 88979-33-3
{bis(η-cyclopentadienyl)(μ-carbonyl)(μ-bis(diphenylphosphinomethane))dirhodium}

Guidance literature:: With triphenyl phosphine; In dichloromethane; a stoich. amount of PPh3 was added to a CH2Cl2 soln. of Rh2Cu-cluster under N2, mixt. was stirred for ca. 30 min at room temp.; evapd., residue was extd. with Et2O, Rh2-complex was isolated from the ext., solid residue was identified as Cu(PPh3)Cl;