2-(2-(2-(-4-azido-2,3,5,6-tetrafluorobenzamido)ethoxy)ethoxy)ethyl 2-bromo-2-methylpropanoate

Base Information

Chemical Name:2-(2-(2-(-4-azido-2,3,5,6-tetrafluorobenzamido)ethoxy)ethoxy)ethyl 2-bromo-2-methylpropanoate
CAS No.:1265905-73-4
Molecular Formula:C₁₇H₁₉BrF₄N₄O₅
Molecular Weight:515.259
Hs Code.:

Synonyms:2-(2-(2-(-4-azido-2,3,5,6-tetrafluorobenzamido)ethoxy)ethoxy)ethyl 2-bromo-2-methylpropanoate

Suppliers and Price of 2-(2-(2-(-4-azido-2,3,5,6-tetrafluorobenzamido)ethoxy)ethoxy)ethyl 2-bromo-2-methylpropanoate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 2-(2-(2-(-4-azido-2,3,5,6-tetrafluorobenzamido)ethoxy)ethoxy)ethyl 2-bromo-2-methylpropanoate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2-(2-(2-(-4-azido-2,3,5,6-tetrafluorobenzamido)ethoxy)ethoxy)ethyl 2-bromo-2-methylpropanoate

There total 4 articles about 2-(2-(2-(-4-azido-2,3,5,6-tetrafluorobenzamido)ethoxy)ethoxy)ethyl 2-bromo-2-methylpropanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.5%

: 20769-85-1
2-bromoisobutyric acid bromide

: 1093346-60-1
4-azido-2,3,5,6-tetrafluoro-N-(2-(2-(2-hydroxyethoxy)ethoxy)ethyl)benzamide

: 1265905-73-4
2-(2-(2-(-4-azido-2,3,5,6-tetrafluorobenzamido)ethoxy)ethoxy)ethyl 2-bromo-2-methylpropanoate

Guidance literature:: With pyridine; In dichloromethane; at 20 ℃; for 5h;
DOI:10.1002/asia.201000569

Reference yield:

: 36629-42-2
methyl pentafluorobenzoate

: 1265905-73-4
2-(2-(2-(-4-azido-2,3,5,6-tetrafluorobenzamido)ethoxy)ethoxy)ethyl 2-bromo-2-methylpropanoate

Guidance literature:: Multi-step reaction with 5 steps

1: sodium azide / water; acetone / 8 h / Reflux

2: water; sodium hydroxide / methanol / 20 °C

3: dicyclohexyl-carbodiimide / dichloromethane / 20 °C

4: triethylamine / acetonitrile / 72 h / 20 °C

5: pyridine / dichloromethane / 5 h / 20 °C

With pyridine; sodium azide; water; triethylamine; dicyclohexyl-carbodiimide; sodium hydroxide; In methanol; dichloromethane; water; acetone; acetonitrile;
DOI:10.1002/asia.201000569

Reference yield:

: 122590-75-4
methyl 4-azidotetrafluorobenzoate

: 1265905-73-4
2-(2-(2-(-4-azido-2,3,5,6-tetrafluorobenzamido)ethoxy)ethoxy)ethyl 2-bromo-2-methylpropanoate

Guidance literature:: Multi-step reaction with 4 steps

1: water; sodium hydroxide / methanol / 20 °C

2: dicyclohexyl-carbodiimide / dichloromethane / 20 °C

3: triethylamine / acetonitrile / 72 h / 20 °C

4: pyridine / dichloromethane / 5 h / 20 °C

With pyridine; water; triethylamine; dicyclohexyl-carbodiimide; sodium hydroxide; In methanol; dichloromethane; acetonitrile;
DOI:10.1002/asia.201000569