8-(2-ethoxyphenyl)-7,8-dihydro-[1,3]dioxolo[4,5-g]quinoline-6(5H)-thione

Base Information

Chemical Name:8-(2-ethoxyphenyl)-7,8-dihydro-[1,3]dioxolo[4,5-g]quinoline-6(5H)-thione
CAS No.:1429518-86-4
Molecular Formula:C₁₈H₁₇NO₃S
Molecular Weight:327.404
Hs Code.:

Synonyms:8-(2-ethoxyphenyl)-7,8-dihydro-[1,3]dioxolo[4,5-g]quinoline-6(5H)-thione

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Chemical Property of 8-(2-ethoxyphenyl)-7,8-dihydro-[1,3]dioxolo[4,5-g]quinoline-6(5H)-thione

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Technology Process of 8-(2-ethoxyphenyl)-7,8-dihydro-[1,3]dioxolo[4,5-g]quinoline-6(5H)-thione

There total 4 articles about 8-(2-ethoxyphenyl)-7,8-dihydro-[1,3]dioxolo[4,5-g]quinoline-6(5H)-thione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 19.0%

: 599151-35-6
8-(2-ethoxyphenyl)-7,8-dihydro-[1,3]dioxolo[4,5-g]quinolin-6-(5H)-one

: 1429518-86-4
8-(2-ethoxyphenyl)-7,8-dihydro-[1,3]dioxolo[4,5-g]quinoline-6(5H)-thione

Guidance literature:: With Lawessons reagent; In toluene; Inert atmosphere; Reflux;

Reference yield:

: C₁₈H₁₉NO₄

: 1429518-86-4
8-(2-ethoxyphenyl)-7,8-dihydro-[1,3]dioxolo[4,5-g]quinoline-6(5H)-thione

Guidance literature:: Multi-step reaction with 2 steps

1: trifluoroacetic acid / 0.5 h / 70 °C / Microwave irradiation

2: Lawessons reagent / toluene / Inert atmosphere; Reflux

With Lawessons reagent; trifluoroacetic acid; In toluene;

Reference yield:

: 69038-81-9
2-ethoxy cinnamic acid

: 1429518-86-4
8-(2-ethoxyphenyl)-7,8-dihydro-[1,3]dioxolo[4,5-g]quinoline-6(5H)-thione

Guidance literature:: Multi-step reaction with 3 steps

1.1: HATU / N,N-dimethyl-formamide / 1 h / 20 °C

1.2: 3 h / 20 °C

2.1: trifluoroacetic acid / 0.5 h / 70 °C / Microwave irradiation

3.1: Lawessons reagent / toluene / Inert atmosphere; Reflux

With Lawessons reagent; HATU; trifluoroacetic acid; In N,N-dimethyl-formamide; toluene;