methyl 3-azido-4-hydroxybenzoate

Base Information

Chemical Name:methyl 3-azido-4-hydroxybenzoate
CAS No.:1393745-17-9
Molecular Formula:C₈H₇N₃O₃
Molecular Weight:193.162
Hs Code.:

Synonyms:methyl 3-azido-4-hydroxybenzoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl 3-azido-4-hydroxybenzoate

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Technology Process of methyl 3-azido-4-hydroxybenzoate

There total 6 articles about methyl 3-azido-4-hydroxybenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: methyl 3-diazo-4-oxocyclohexa-1,5-diene-1-carboxylate

: 1393745-17-9
methyl 3-azido-4-hydroxybenzoate

Guidance literature:: With Caswell No_. 744A; 2-methoxy-ethanol; at 20 ℃; for 0.0833333h; Inert atmosphere;
DOI:10.1002/ejoc.202200307

Reference yield: 87.0%

: 67-56-1
methanol

: 1393745-16-8
3-azido-4-hydroxybenzoate

: 1393745-17-9
methyl 3-azido-4-hydroxybenzoate

Guidance literature:: With thionyl chloride; at 0 - 20 ℃; for 8h;
DOI:10.1016/j.bmcl.2012.06.017

Reference yield: 74.0%

: 99-76-3,156291-94-0
methyl 4-hydroxylbenzoate

: 1393745-17-9
methyl 3-azido-4-hydroxybenzoate

Guidance literature:: methyl 4-hydroxylbenzoate; With N,N′-1,3-bis(2,6-diisopropylphenyl)-2-chloroimidazolium chloride; diisopropylamine; In 1,2-dimethoxyethane; 2-methoxy-ethanol; at 23 ℃; for 1h; Inert atmosphere;

With sodium azide; In 1,2-dimethoxyethane; 2-methoxy-ethanol; acetonitrile; at 23 ℃; Inert atmosphere;
DOI:10.1002/ejoc.201900967