(Z)-3-{2-[(Z)-1-methyl-3-oxo-3-phenyl-1-propenylamino]ethyl amino}-1-phenyl-2-buten-1-one

Base Information

Chemical Name:(Z)-3-{2-[(Z)-1-methyl-3-oxo-3-phenyl-1-propenylamino]ethyl amino}-1-phenyl-2-buten-1-one
CAS No.:56570-49-1
Molecular Formula:C₂₂H₂₄N₂O₂
Molecular Weight:348.445
Hs Code.:

Synonyms:(Z)-3-{2-[(Z)-1-methyl-3-oxo-3-phenyl-1-propenylamino]ethyl amino}-1-phenyl-2-buten-1-one

Suppliers and Price of (Z)-3-{2-[(Z)-1-methyl-3-oxo-3-phenyl-1-propenylamino]ethyl amino}-1-phenyl-2-buten-1-one

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (Z)-3-{2-[(Z)-1-methyl-3-oxo-3-phenyl-1-propenylamino]ethyl amino}-1-phenyl-2-buten-1-one

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Technology Process of (Z)-3-{2-[(Z)-1-methyl-3-oxo-3-phenyl-1-propenylamino]ethyl amino}-1-phenyl-2-buten-1-one

There total 1 articles about (Z)-3-{2-[(Z)-1-methyl-3-oxo-3-phenyl-1-propenylamino]ethyl amino}-1-phenyl-2-buten-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 107-15-3,85404-18-8
ethylenediamine

: 93-91-4
1-phenylbutan-1,3-dione

: 56570-49-1
(Z)-3-{2-[(Z)-1-methyl-3-oxo-3-phenyl-1-propenylamino]ethyl amino}-1-phenyl-2-buten-1-one

Guidance literature:: With β‐cyclodextrin; In water; at 20 ℃; for 0.5h; chemospecific reaction;
DOI:10.1002/jccs.200800032

Reference yield: 85.0%

: 998-40-3
tributylphosphine

: 56570-49-1
(Z)-3-{2-[(Z)-1-methyl-3-oxo-3-phenyl-1-propenylamino]ethyl amino}-1-phenyl-2-buten-1-one

: sodium perchlorate

: 6147-53-1
cobalt(II) diacetate tetrahydrate

: (bis(benzoylacetone)ethylenediimino)(tributylphosphine)cobalt(III) perchlorate monohydrate

Guidance literature:: With air; In methanol; to stirred soln. of Schiff base in CH3OH cobalt salt and phosphine added, air blowed into soln. for 2 h, soln. filtered, NaClO4 added; crystals filtered, washed (CH3OH), recrystd. from CH3OH, dried (vac., 343 K); elem. anal.;
DOI:10.1080/15533170500225441

Reference yield: 75.0%

: 56570-49-1
(Z)-3-{2-[(Z)-1-methyl-3-oxo-3-phenyl-1-propenylamino]ethyl amino}-1-phenyl-2-buten-1-one

: sodium perchlorate

: 6147-53-1
cobalt(II) diacetate tetrahydrate

: 554-70-1
triethylphosphine

: (bis(benzoylacetone)ethylenediimino)(triethylphosphine)cobalt(III) perchlorate monohydrate

Guidance literature:: With air; In methanol; to stirred soln. of Schiff base in CH3OH cobalt salt and phosphine added, air blowed into soln. for 2 h, soln. filtered, NaClO4 added; crystals filtered, washed (CH3OH), recrystd. from CH3OH, dried (vac., 343 K); elem. anal.;
DOI:10.1080/15533170500225441