5-(1,1-dioxo-[1,2]thiazinan-2-yl)-N,N-dipropylisophthalamic acid methyl ester

Base Information

Chemical Name:5-(1,1-dioxo-[1,2]thiazinan-2-yl)-N,N-dipropylisophthalamic acid methyl ester
CAS No.:1349188-02-8
Molecular Formula:C₁₉H₂₈N₂O₅S
Molecular Weight:396.508
Hs Code.:

Synonyms:5-(1,1-dioxo-[1,2]thiazinan-2-yl)-N,N-dipropylisophthalamic acid methyl ester

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Chemical Property of 5-(1,1-dioxo-[1,2]thiazinan-2-yl)-N,N-dipropylisophthalamic acid methyl ester

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Technology Process of 5-(1,1-dioxo-[1,2]thiazinan-2-yl)-N,N-dipropylisophthalamic acid methyl ester

There total 3 articles about 5-(1,1-dioxo-[1,2]thiazinan-2-yl)-N,N-dipropylisophthalamic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 911790-36-8
5-(1,1-dioxo-[1,2]thiazinan-2-yl)isophthalic acid monomethyl ester

: 142-84-7
di-n-propylamine

: 1349188-02-8
5-(1,1-dioxo-[1,2]thiazinan-2-yl)-N,N-dipropylisophthalamic acid methyl ester

Guidance literature:: 5-(1,1-dioxo-[1,2]thiazinan-2-yl)isophthalic acid monomethyl ester; With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; for 1h; Inert atmosphere;

di-n-propylamine; In dichloromethane; at 20 ℃; Inert atmosphere;
DOI:10.1021/ml4004952

Reference yield:

: 99-27-4
dimethyl 5-aminoisophthalate

: 1349188-02-8
5-(1,1-dioxo-[1,2]thiazinan-2-yl)-N,N-dipropylisophthalamic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: pyridine

1.2: 60 °C

1.3: 20 °C

2.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 1 h / Inert atmosphere

2.2: 20 °C / Inert atmosphere

With pyridine; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane;
DOI:10.1021/ml4004952

Reference yield:

: 911790-35-7
C₁₄H₁₇NO₆S

: 1349188-02-8
5-(1,1-dioxo-[1,2]thiazinan-2-yl)-N,N-dipropylisophthalamic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydroxide / water; methanol / 20 °C

2.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 1 h / Inert atmosphere

2.2: 20 °C / Inert atmosphere

With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; sodium hydroxide; In methanol; dichloromethane; water;
DOI:10.1021/ml4004952