C₂₃H₁₉F₃O₄

Base Information

Chemical Name:C₂₃H₁₉F₃O₄
CAS No.:1335557-40-8
Molecular Formula:C₂₃H₁₉F₃O₄
Molecular Weight:416.397
Hs Code.:

C<sub>23</sub>H<sub>19</sub>F<sub>3</sub>O<sub>4</sub>

Synonyms:C₂₃H₁₉F₃O₄

Suppliers and Price of C₂₃H₁₉F₃O₄

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₂₃H₁₉F₃O₄

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₂₃H₁₉F₃O₄

There total 12 articles about C₂₃H₁₉F₃O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1254348-96-3
C₂₃H₁₇F₃O₄

: 1335557-40-8
C₂₃H₁₉F₃O₄

Guidance literature:: With methanol; sodium tetrahydroborate; for 2h;

Reference yield:

: 877149-05-8
4-bromo-2-methoxy-6-methyl-benzonitrile

: 1335557-40-8
C₂₃H₁₉F₃O₄

Guidance literature:: Multi-step reaction with 11 steps

1.1: diisobutylaluminium hydride / toluene; tetrahydrofuran / -78 - 20 °C

1.2: 0 - 20 °C

2.1: 2-methyl-but-2-ene; water; sodium chlorite; sodium dihydrogenphosphate / tert-butyl alcohol / 0.5 h / 20 °C

2.2: pH 1

3.1: oxalyl dichloride / N,N-dimethyl-formamide / dichloromethane / 0.5 h / 20 °C

4.1: dmap; triethylamine / dichloromethane / 1 h / 20 °C

5.1: potassium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,4-dioxane; water / 19 h / Inert atmosphere; Reflux

6.1: ozone; oxygen / dichloromethane / -78 °C

6.2: -78 - 25 °C

7.1: bromine; acetic acid / 1 h / 20 °C

8.1: boron tribromide / dichloromethane / 1.5 h / -78 - 25 °C

9.1: potassium carbonate / N,N-dimethyl-formamide / 2 h / 20 °C

10.1: copper(l) iodide / N,N-dimethyl-formamide / 20 h / 100 °C / Sealed

11.1: sodium tetrahydroborate; methanol / 2 h

With methanol; dmap; sodium chlorite; sodium tetrahydroborate; sodium dihydrogenphosphate; copper(l) iodide; 2-methyl-but-2-ene; oxalyl dichloride; water; bromine; oxygen; boron tribromide; diisobutylaluminium hydride; potassium carbonate; ozone; acetic acid; triethylamine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; N,N-dimethyl-formamide; In tetrahydrofuran; 1,4-dioxane; dichloromethane; water; N,N-dimethyl-formamide; toluene; tert-butyl alcohol;

Reference yield:

: 348169-39-1
4-bromo-2-methoxy-6-methyl-phenylamine

: 1335557-40-8
C₂₃H₁₉F₃O₄

Guidance literature:: Multi-step reaction with 12 steps

1.1: hydrogenchloride; sodium nitrite / water / 0.5 h / 0 °C

1.3: 4 h / 0 - 50 °C

2.1: diisobutylaluminium hydride / toluene; tetrahydrofuran / -78 - 20 °C

2.2: 0 - 20 °C

3.1: 2-methyl-but-2-ene; water; sodium chlorite; sodium dihydrogenphosphate / tert-butyl alcohol / 0.5 h / 20 °C

3.2: pH 1

4.1: oxalyl dichloride / N,N-dimethyl-formamide / dichloromethane / 0.5 h / 20 °C

5.1: dmap; triethylamine / dichloromethane / 1 h / 20 °C

6.1: potassium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,4-dioxane; water / 19 h / Inert atmosphere; Reflux

7.1: ozone; oxygen / dichloromethane / -78 °C

7.2: -78 - 25 °C

8.1: bromine; acetic acid / 1 h / 20 °C

9.1: boron tribromide / dichloromethane / 1.5 h / -78 - 25 °C

10.1: potassium carbonate / N,N-dimethyl-formamide / 2 h / 20 °C

11.1: copper(l) iodide / N,N-dimethyl-formamide / 20 h / 100 °C / Sealed

12.1: sodium tetrahydroborate; methanol / 2 h

With hydrogenchloride; methanol; dmap; sodium chlorite; sodium tetrahydroborate; sodium dihydrogenphosphate; copper(l) iodide; 2-methyl-but-2-ene; oxalyl dichloride; water; bromine; oxygen; boron tribromide; diisobutylaluminium hydride; potassium carbonate; ozone; acetic acid; triethylamine; sodium nitrite; tetrakis(triphenylphosphine) palladium⁽⁰⁾; N,N-dimethyl-formamide; In tetrahydrofuran; 1,4-dioxane; dichloromethane; water; N,N-dimethyl-formamide; toluene; tert-butyl alcohol;