phenyl 4-ethenyl-2-methoxy-6-methylbenzoate

Base Information

Chemical Name:phenyl 4-ethenyl-2-methoxy-6-methylbenzoate
CAS No.:1254348-93-0
Molecular Formula:C₁₇H₁₆O₃
Molecular Weight:268.312
Hs Code.:

Synonyms:phenyl 4-ethenyl-2-methoxy-6-methylbenzoate

Suppliers and Price of phenyl 4-ethenyl-2-methoxy-6-methylbenzoate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of phenyl 4-ethenyl-2-methoxy-6-methylbenzoate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of phenyl 4-ethenyl-2-methoxy-6-methylbenzoate

There total 7 articles about phenyl 4-ethenyl-2-methoxy-6-methylbenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 877149-08-1
4-bromo-2-methoxy-6-methyl-benzoic acid

: 1254348-93-0
phenyl 4-ethenyl-2-methoxy-6-methylbenzoate

Guidance literature:: Multi-step reaction with 3 steps

1: oxalyl dichloride / N,N-dimethyl-formamide / dichloromethane / 0.5 h / 20 °C

2: dmap; triethylamine / dichloromethane / 1 h / 20 °C

3: potassium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,4-dioxane; water / 19 h / Inert atmosphere; Reflux

With dmap; oxalyl dichloride; potassium carbonate; triethylamine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; N,N-dimethyl-formamide; In 1,4-dioxane; dichloromethane; water;

Reference yield:

: 877149-05-8
4-bromo-2-methoxy-6-methyl-benzonitrile

: 1254348-93-0
phenyl 4-ethenyl-2-methoxy-6-methylbenzoate

Guidance literature:: Multi-step reaction with 5 steps

1.1: diisobutylaluminium hydride / toluene; tetrahydrofuran / -78 - 20 °C

1.2: 0 - 20 °C

2.1: 2-methyl-but-2-ene; water; sodium chlorite; sodium dihydrogenphosphate / tert-butyl alcohol / 0.5 h / 20 °C

2.2: pH 1

3.1: oxalyl dichloride / N,N-dimethyl-formamide / dichloromethane / 0.5 h / 20 °C

4.1: dmap; triethylamine / dichloromethane / 1 h / 20 °C

5.1: potassium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,4-dioxane; water / 19 h / Inert atmosphere; Reflux

With dmap; sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene; oxalyl dichloride; water; diisobutylaluminium hydride; potassium carbonate; triethylamine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; N,N-dimethyl-formamide; In tetrahydrofuran; 1,4-dioxane; dichloromethane; water; toluene; tert-butyl alcohol;

Reference yield:

: 1244949-43-6
4-bromo-2-methoxy-6-methyl-benzaldehyde

: 1254348-93-0
phenyl 4-ethenyl-2-methoxy-6-methylbenzoate

Guidance literature:: Multi-step reaction with 4 steps

1.1: 2-methyl-but-2-ene; water; sodium chlorite; sodium dihydrogenphosphate / tert-butyl alcohol / 0.5 h / 20 °C

1.2: pH 1

2.1: oxalyl dichloride / N,N-dimethyl-formamide / dichloromethane / 0.5 h / 20 °C

3.1: dmap; triethylamine / dichloromethane / 1 h / 20 °C

4.1: potassium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,4-dioxane; water / 19 h / Inert atmosphere; Reflux

With dmap; sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene; oxalyl dichloride; water; potassium carbonate; triethylamine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; N,N-dimethyl-formamide; In 1,4-dioxane; dichloromethane; water; tert-butyl alcohol;