5-CHLORO-3-IODO-1H-PYRROLO[2,3-B]PYRIDINE

Base Information

• Chemical Name: 5-CHLORO-3-IODO-1H-PYRROLO[2,3-B]PYRIDINE
• CAS No.: 900514-08-1
• Molecular Formula: C7H4 Cl I N2
• Molecular Weight: 278.48
• Hs Code.: 2933990090
• Mol file: 900514-08-1.mol

Synonyms:5-CHLORO-3-IODO-1H-PYRROLO[2,3-B]PYRIDINE;1H-Pyrrolo[2,3-b]pyridine, 5-chloro-3-iodo-

Chemical Property of 5-CHLORO-3-IODO-1H-PYRROLO[2,3-B]PYRIDINE

Chemical Property:

• Melting Point: 228-229掳C
• Refractive Index: 1.784
• PSA: 28.68000
• Density: 2.156g/cm³
• LogP: 2.82090
• Storage Temp.: under inert gas (nitrogen or Argon) at 2–8 °C

Purity/Quality:

99%, ^*data from raw suppliers

5-Chloro-3-iodo-1H-pyrrolo[2,3-b]pyridine Aldrich ^*data from reagent suppliers

Safty Information:

• Hazard Codes: Xi

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 5-CHLORO-3-IODO-1H-PYRROLO[2,3-B]PYRIDINE

There total 1 articles about 5-CHLORO-3-IODO-1H-PYRROLO[2,3-B]PYRIDINE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

5-chloro-1H-pyrrolo[2,3-b]pyridine (866546-07-8) → 5-chloro-3-iodo-1H-pyrrolo[2,3-b]pyridine (900514-08-1)

Guidance literature:

With pyridine; Iodine monochloride; In dichloromethane; at 20 ℃; for 2.33333h; Inert atmosphere;

Reference yield: 70.0%

5-chloro-3-iodo-1H-pyrrolo[2,3-b]pyridine (900514-08-1) + p-toluenesulfonyl chloride (98-59-9) → 5-chloro-3-iodo-1-tosyl-1H-pyrrolo[2,3-b]pyridine (1241675-24-0)

Guidance literature:

With caesium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 4h;

Reference yield:

5-chloro-3-iodo-1H-pyrrolo[2,3-b]pyridine (900514-08-1) + benzenesulfonyl chloride (98-09-9) → 1-benzenesulfonyl-5-chloro-3-iodo-1H-pyrrolo[2,3-b]pyridine (1001414-09-0)

Guidance literature:

With sodium hydride; In N,N-dimethyl-formamide; mineral oil; at 0 - 20 ℃; for 15h;

upstream raw materials:

5-chloro-1H-pyrrolo[2,3-b]pyridine

Downstream raw materials:

(1-benzenesulfonyl-5-chloro-1H-pyrrolo[2,3-b]pyridin-3-yl)(2-methylsulfanylpyrimidin-5-yl)methanol

1-benzenesulfonyl-5-chloro-3-(2-methylsulfanylpyrimidin-5-ylmethyl)-1H-pyrrolo[2,3-b]pyridine

1-benzenesulfonyl-5-chloro-3-(2-methanesulfonylpyrimidin-5-ylmethyl)-1H-pyrrolo[2,3-b]pyridine

5-(1-benzenesulfonyl-5-chloro-1H-pyrrolo[2,3-b]pyridin-3-ylmethyl)-4-chlorothiazol-2-ylamine

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