N-[(1,1-dimethylethoxy)carbonyl]-3-[3-formyl-4-(phenylmethoxy)phenyl]-L-alanine

Base Information

Chemical Name:N-[(1,1-dimethylethoxy)carbonyl]-3-[3-formyl-4-(phenylmethoxy)phenyl]-L-alanine
CAS No.:186689-04-3
Molecular Formula:C₂₂H₂₅NO₆
Molecular Weight:399.444
Hs Code.:

Synonyms:N-[(1,1-dimethylethoxy)carbonyl]-3-[3-formyl-4-(phenylmethoxy)phenyl]-L-alanine

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Chemical Property of N-[(1,1-dimethylethoxy)carbonyl]-3-[3-formyl-4-(phenylmethoxy)phenyl]-L-alanine

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Technology Process of N-[(1,1-dimethylethoxy)carbonyl]-3-[3-formyl-4-(phenylmethoxy)phenyl]-L-alanine

There total 7 articles about N-[(1,1-dimethylethoxy)carbonyl]-3-[3-formyl-4-(phenylmethoxy)phenyl]-L-alanine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 100-39-0
benzyl bromide

: 186689-03-2
2-(tert-butoxycarbonylamino)-3-(3-formyl-4-hydroxyphenyl)propanoic acid

: 186689-04-3
N-[(1,1-dimethylethoxy)carbonyl]-3-[3-formyl-4-(phenylmethoxy)phenyl]-L-alanine

Guidance literature:: With potassium carbonate; In methanol; chloroform; for 4h; Heating;
DOI:10.1021/jo962099r

Reference yield:

: 60-18-4,18875-48-4,25619-78-7,30704-25-7
L-tyrosine

: 186689-04-3
N-[(1,1-dimethylethoxy)carbonyl]-3-[3-formyl-4-(phenylmethoxy)phenyl]-L-alanine

Guidance literature:: Multi-step reaction with 3 steps

2: NaOH / H₂O

3: K₂CO₃

With sodium hydroxide; potassium carbonate; In water;
DOI:10.1021/jo9902751

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 186689-04-3
N-[(1,1-dimethylethoxy)carbonyl]-3-[3-formyl-4-(phenylmethoxy)phenyl]-L-alanine

Guidance literature:: Multi-step reaction with 3 steps

1: 92 percent / Et₃N / dioxane; H₂O / 18 h / Ambient temperature

2: 66 percent Turnov_. / NaOH / H₂O / 6.5 h

3: 71 percent / K₂CO₃ / CHCl₃; methanol / 4 h / Heating

With sodium hydroxide; potassium carbonate; triethylamine; In 1,4-dioxane; methanol; chloroform; water;
DOI:10.1021/jo962099r