2,5-DIMETHYLCYCLOHEXANONE

Base Information

• Chemical Name: 2,5-DIMETHYLCYCLOHEXANONE
• CAS No.: 932-51-4
• Molecular Formula: C8H14 O
• Molecular Weight: 126.199
• Mol file: 932-51-4.mol

Synonyms:2,5-Dimethylcyclohexanone

Chemical Property of 2,5-DIMETHYLCYCLOHEXANONE

Chemical Property:

• Refractive Index: 1.4440-1.4480
• Boiling Point: 80 °C / 30mmHg
• PSA: 17.07000
• Density: 0.91
• LogP: 2.01160
• Storage Temp.: Refrigerator

Purity/Quality:

98% ^*data from raw suppliers

2,5-Dimethylcyclohexanone ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2,5-DIMETHYLCYCLOHEXANONE

There total 61 articles about 2,5-DIMETHYLCYCLOHEXANONE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

2,5-dimethylcyclohexanol (3809-32-3) → 2,5-dimethylcyclohexanone (932-51-4)

Guidance literature:

With pyridinium chlorochromate; In dichloromethane;

DOI:10.1021/jo000956s

Reference yield: 84.0%

2,5-dimethylcyclohexanone oxime (4500-14-5) → 2,5-dimethylcyclohexanone (932-51-4)

Guidance literature:

With KMnO₄/alumina; In diethyl ether; at 0 ℃; for 6h;

DOI:10.1016/S0040-4039(01)00850-4

Reference yield: 68.0%

6-methylcyclohex-2-en-1-one (6610-21-5) + methyllithium (917-54-4) → 2,5-dimethylcyclohexanone (932-51-4)

Guidance literature:

With methylandrostenediol; In diethyl ether; hexane; toluene; at -78 ℃; for 0.5h;

DOI:10.1016/S0040-4039(00)96824-2

upstream raw materials:

2,5-Dimethylphenol

methyl magnesium iodide

2-chloro-5-methyl-cyclohexanone

diethyl ether

Downstream raw materials:

2,5-dimethylcyclohexanol

3,6-dimethyl-1,2-cyclohexanedione

2-chloro-3,6-dimethyl-cyclohexanone

1-Phenyl-2,5-dimethylcyclohexanol

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