n'-Benzylidene-4-chlorobenzohydrazide

Base Information

Chemical Name:n'-Benzylidene-4-chlorobenzohydrazide
CAS No.:31061-81-1
Molecular Formula:C14H11 Cl N2 O
Molecular Weight:258.707
Hs Code.:
NSC Number:148186
Mol file:31061-81-1.mol

Synonyms:n'-benzylidene-4-chlorobenzohydrazide;4-chloro-N'-[(E)-phenylmethylidene]benzohydrazide;NSC148186;31061-81-1;STK236050;AKOS001022012;NSC-148186;AB00722920-01;SR-01000107698;SR-01000107698-1;Z49577934

Suppliers and Price of n'-Benzylidene-4-chlorobenzohydrazide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of n'-Benzylidene-4-chlorobenzohydrazide

Chemical Property:

XLogP3:3.2
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:3
Exact Mass:258.0559907
Heavy Atom Count:18
Complexity:292

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)C=NNC(=O)C2=CC=C(C=C2)Cl
Isomeric SMILES:C1=CC=C(C=C1)/C=N/NC(=O)C2=CC=C(C=C2)Cl

Technology Process of n'-Benzylidene-4-chlorobenzohydrazide

There total 6 articles about n'-Benzylidene-4-chlorobenzohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 100-52-7
benzaldehyde

: 536-40-3
4-chlorobenzoic acid hydrazide

: 31061-81-1
2-(phenylmethylene)-(4-chloro)benzoic acid hydrazide

Guidance literature:: ammonium cerium(IV) nitrate; In ethanol; for 0.5h; Heating;
DOI:10.1016/j.tetlet.2006.07.127

Reference yield:

: 74-11-3
para-chlorobenzoic acid

: 31061-81-1
2-(phenylmethylene)-(4-chloro)benzoic acid hydrazide

Guidance literature:: Multi-step reaction with 3 steps

1: sulfuric acid / 12 h / Reflux

2: hydrazine hydrate / ethanol / 3 h / Reflux

3: acetic acid / ethanol / 3 h / Reflux

With sulfuric acid; hydrazine hydrate; acetic acid; In ethanol;
DOI:10.21608/ejchem.2021.53056.3260

Reference yield:

: 1126-46-1
Methyl 4-chlorobenzoate

: 31061-81-1
2-(phenylmethylene)-(4-chloro)benzoic acid hydrazide

Guidance literature:: Multi-step reaction with 2 steps

1: hydrazine hydrate / ethanol / 3 h / Reflux

2: acetic acid / ethanol / 3 h / Reflux

With hydrazine hydrate; acetic acid; In ethanol;
DOI:10.21608/ejchem.2021.53056.3260