C₁₃H₁₉NO₅S

Base Information

Chemical Name:C₁₃H₁₉NO₅S
CAS No.:1418318-99-6
Molecular Formula:C₁₃H₁₉NO₅S
Molecular Weight:301.364
Hs Code.:

C<sub>13</sub>H<sub>19</sub>NO<sub>5</sub>S

Synonyms:C₁₃H₁₉NO₅S

Suppliers and Price of C₁₃H₁₉NO₅S

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₁₃H₁₉NO₅S

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₁₃H₁₉NO₅S

There total 3 articles about C₁₃H₁₉NO₅S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 856408-80-5
(R)-N-ethyl-N-methylcarbamic acid-3-(1-hydroxyethyl)phenyl ester

: 124-63-0
methanesulfonyl chloride

: 1418318-99-6
C₁₃H₁₉NO₅S

Guidance literature:: With triethylamine; In dichloromethane; at 0 ℃; for 1.5h; Inert atmosphere;
DOI:10.1021/jo9027374

Reference yield:

: 121-71-1
3-Hydroxyacetophenone

: 1418318-99-6
C₁₃H₁₉NO₅S

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium carbonate / ethyl acetate / Inert atmosphere; Reflux; Large scale

2.1: hydrogen; sodium t-butanolate; C₅₂H₆₇ClIrN₂P / ethanol / 20 - 55 °C / 22502.3 - 24002.4 Torr / Autoclave; Inert atmosphere; Schlenk technique; Large scale

3.1: triethylamine / tetrahydrofuran / 0.75 h / 0 - 20 °C / Inert atmosphere; Large scale

3.2: 2 h / 0 - 20 °C / Inert atmosphere; Large scale

With C₅₂H₆₇ClIrN₂P; hydrogen; potassium carbonate; triethylamine; sodium t-butanolate; In tetrahydrofuran; ethanol; ethyl acetate;
DOI:10.1021/op3003147

Reference yield:

: 855300-09-3
1-(N-ethyl-N-methylaminocarbonyloxy)-3-acetylbenzene

: 1418318-99-6
C₁₃H₁₉NO₅S

Guidance literature:: Multi-step reaction with 2 steps

1.1: hydrogen; sodium t-butanolate; C₅₂H₆₇ClIrN₂P / ethanol / 20 - 55 °C / 22502.3 - 24002.4 Torr / Autoclave; Inert atmosphere; Schlenk technique; Large scale

2.1: triethylamine / tetrahydrofuran / 0.75 h / 0 - 20 °C / Inert atmosphere; Large scale

2.2: 2 h / 0 - 20 °C / Inert atmosphere; Large scale

With C₅₂H₆₇ClIrN₂P; hydrogen; triethylamine; sodium t-butanolate; In tetrahydrofuran; ethanol;
DOI:10.1021/op3003147