C₂₄H₃₀INO₁₂

Base Information

Chemical Name:C₂₄H₃₀INO₁₂
CAS No.:1607459-34-6
Molecular Formula:C₂₄H₃₀INO₁₂
Molecular Weight:651.406
Hs Code.:

C<sub>24</sub>H<sub>30</sub>INO<sub>12</sub>

Synonyms:C₂₄H₃₀INO₁₂

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Chemical Property of C₂₄H₃₀INO₁₂

Chemical Property:

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Technology Process of C₂₄H₃₀INO₁₂

There total 4 articles about C₂₄H₃₀INO₁₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 67-56-1
methanol

: 1620208-08-3
C₂₃H₂₈INO₁₂

: 1607459-34-6
C₂₄H₃₀INO₁₂

Guidance literature:: With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In dichloromethane; at 0 - 25 ℃; for 20h; Inert atmosphere;
DOI:10.1021/jo500465m

Reference yield:

: 1607459-23-3
C₂₉H₄₂INO₁₂Si

: 1607459-34-6
C₂₄H₃₀INO₁₂

Guidance literature:: Multi-step reaction with 2 steps

1: trimethylsilyl trifluoromethanesulfonate / dichloromethane / 3 h / -78 - 0 °C / Molecular sieve; Inert atmosphere

2: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; dmap / dichloromethane / 20 h / 0 - 25 °C / Inert atmosphere

With dmap; trimethylsilyl trifluoromethanesulfonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In dichloromethane;
DOI:10.1021/jo500465m

Reference yield:

: 2873-29-2
D-glucal triacetate

: 1607459-34-6
C₂₄H₃₀INO₁₂

Guidance literature:: Multi-step reaction with 3 steps

1: cetyltrimethylammonim bromide; magnesium sulfate; potassium iodide / dichloromethane / 6 h / 0 - 25 °C / Inert atmosphere

2: trimethylsilyl trifluoromethanesulfonate / dichloromethane / 3 h / -78 - 0 °C / Molecular sieve; Inert atmosphere

3: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; dmap / dichloromethane / 20 h / 0 - 25 °C / Inert atmosphere

With dmap; trimethylsilyl trifluoromethanesulfonate; cetyltrimethylammonim bromide; magnesium sulfate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; potassium iodide; In dichloromethane;
DOI:10.1021/jo500465m