N-Benzyloxycarbonyl-glycyl-N-(2-benzoyl-4-chlor-phenyl)-N-methyl-glycinamid

Base Information

Chemical Name:N-Benzyloxycarbonyl-glycyl-N-(2-benzoyl-4-chlor-phenyl)-N-methyl-glycinamid
CAS No.:59180-10-8
Molecular Formula:C₂₆H₂₄ClN₃O₅
Molecular Weight:493.947
Hs Code.:

Synonyms:N-Benzyloxycarbonyl-glycyl-N-(2-benzoyl-4-chlor-phenyl)-N-methyl-glycinamid

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-Benzyloxycarbonyl-glycyl-N-(2-benzoyl-4-chlor-phenyl)-N-methyl-glycinamid

Chemical Property:

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Technology Process of N-Benzyloxycarbonyl-glycyl-N-(2-benzoyl-4-chlor-phenyl)-N-methyl-glycinamid

There total 4 articles about N-Benzyloxycarbonyl-glycyl-N-(2-benzoyl-4-chlor-phenyl)-N-methyl-glycinamid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.3%

: 59180-31-3
{[({[4-Chloro-2-(hydroxy-phenyl-methyl)-phenyl]-methyl-carbamoyl}-methyl)-carbamoyl]-methyl}-carbamic acid benzyl ester

: 59180-10-8
N-Benzyloxycarbonyl-glycyl-N-(2-benzoyl-4-chlor-phenyl)-N-methyl-glycinamid

Guidance literature:: With jones reagent; In acetone;
DOI:10.1021/jm00181a013

Reference yield:

: 2566-19-0
CbzGlyGly

: 59180-10-8
N-Benzyloxycarbonyl-glycyl-N-(2-benzoyl-4-chlor-phenyl)-N-methyl-glycinamid

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) HMPA, SOCl₂ / 1.) CH₃CN, -18 deg C, 30 min, 2.) CH₃CN, -20 deg C, overnight

2: 90.3 percent / Jones reagent / acetone

With N,N,N,N,N,N-hexamethylphosphoric triamide; thionyl chloride; jones reagent; In acetone;
DOI:10.1021/jm00181a013

Reference yield:

: 13386-35-1
2-methylamino-5-chlorobenzhydrol

: 59180-10-8
N-Benzyloxycarbonyl-glycyl-N-(2-benzoyl-4-chlor-phenyl)-N-methyl-glycinamid

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) HMPA, SOCl₂ / 1.) CH₃CN, -18 deg C, 30 min, 2.) CH₃CN, -20 deg C, overnight

2: 90.3 percent / Jones reagent / acetone

With N,N,N,N,N,N-hexamethylphosphoric triamide; thionyl chloride; jones reagent; In acetone;
DOI:10.1021/jm00181a013