<(4-Bromophenyl)azo>pyrrolidine

Base Information

Chemical Name:<(4-Bromophenyl)azo>pyrrolidine
CAS No.:250160-26-0
Molecular Formula:C₁₀H₁₂BrN₃
Molecular Weight:254.129
Hs Code.:

Synonyms:<(4-Bromophenyl)azo>pyrrolidine

Suppliers and Price of <(4-Bromophenyl)azo>pyrrolidine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of <(4-Bromophenyl)azo>pyrrolidine

Chemical Property:

Purity/Quality:: 99% ^*data from raw suppliers

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Technology Process of <(4-Bromophenyl)azo>pyrrolidine

There total 1 articles about <(4-Bromophenyl)azo>pyrrolidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 123-75-1
pyrrolidine

: 106-40-1
4-bromo-aniline

: 250160-26-0
<(4-Bromophenyl)azo>pyrrolidine

Guidance literature:: 4-bromo-aniline; With hydrogenchloride; sodium nitrite; In water; acetonitrile; at -5 - 0 ℃; for 0.5h;

pyrrolidine; With potassium carbonate; In water; acetonitrile; at 0 ℃;
DOI:10.1002/anie.201301742

Reference yield: 87.0%

: 501-65-5
diphenyl acetylene

: 250160-26-0
<(4-Bromophenyl)azo>pyrrolidine

: 1259224-11-7
5-bromo-2,3-diphenyl-1H-indole

Guidance literature:: With silver hexafluoroantimonate; dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; copper(II) acetate monohydrate; In methanol; at 90 ℃; regioselective reaction; Schlenk technique; Inert atmosphere;
DOI:10.1002/anie.201301742

Reference yield: 63.0%

: 188290-36-0,8014-23-1,25233-34-5
thiophene

: 250160-26-0
<(4-Bromophenyl)azo>pyrrolidine

: (E)-1-((4-(thiophen-2-yl)phenyl)diazenyl)pyrrolidine

Guidance literature:: With palladium diacetate; potassium carbonate; triphenylphosphine; Trimethylacetic acid; In N,N-dimethyl-formamide; at 110 ℃; for 12h; Schlenk technique; Inert atmosphere;
DOI:10.1021/acs.joc.7b00054