Technology Process of C47H30N6
There total 6 articles about C47H30N6 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
sodium t-butanolate;
tris-(dibenzylideneacetone)dipalladium(0); DavePhos;
In
toluene;
at 120 ℃;
for 24h;
Reflux;
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: ethanol / 2 h / 100 °C
2.1: hydrazine hydrate / 2 h / 100 °C
3.1: sodium nitrite; acetic acid / water / 0 °C
4.1: xylene / 5 h / 140 °C / Inert atmosphere; Reflux
5.1: hydrogen / palladium on carbon / ethanol / 6 h
5.2: 24 h / 100 °C / Reflux
6.1: sodium t-butanolate / DavePhos; tris-(dibenzylideneacetone)dipalladium(0) / toluene / 24 h / 120 °C / Reflux
With
hydrogen; hydrazine hydrate; acetic acid; sodium t-butanolate; sodium nitrite;
tris-(dibenzylideneacetone)dipalladium(0); palladium on carbon; DavePhos;
In
ethanol; water; toluene; xylene;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: sodium nitrite; acetic acid / water / 0 °C
2.1: xylene / 5 h / 140 °C / Inert atmosphere; Reflux
3.1: hydrogen / palladium on carbon / ethanol / 6 h
3.2: 24 h / 100 °C / Reflux
4.1: sodium t-butanolate / DavePhos; tris-(dibenzylideneacetone)dipalladium(0) / toluene / 24 h / 120 °C / Reflux
With
hydrogen; acetic acid; sodium t-butanolate; sodium nitrite;
tris-(dibenzylideneacetone)dipalladium(0); palladium on carbon; DavePhos;
In
ethanol; water; toluene; xylene;