2-(N-morpholinyl)-5-(alpha-cyclopropylcarbonyl-2-fluorobenzyl)-4.5.6.7-tetrahydro-thieno-[3,2-c]pyridine

Base Information

Chemical Name:2-(N-morpholinyl)-5-(alpha-cyclopropylcarbonyl-2-fluorobenzyl)-4.5.6.7-tetrahydro-thieno-[3,2-c]pyridine
CAS No.:1333429-06-3
Molecular Formula:C₂₂H₂₅FN₂O₂S
Molecular Weight:400.517
Hs Code.:

Synonyms:2-(N-morpholinyl)-5-(alpha-cyclopropylcarbonyl-2-fluorobenzyl)-4.5.6.7-tetrahydro-thieno-[3,2-c]pyridine

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Chemical Property of 2-(N-morpholinyl)-5-(alpha-cyclopropylcarbonyl-2-fluorobenzyl)-4.5.6.7-tetrahydro-thieno-[3,2-c]pyridine

Chemical Property:

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Technology Process of 2-(N-morpholinyl)-5-(alpha-cyclopropylcarbonyl-2-fluorobenzyl)-4.5.6.7-tetrahydro-thieno-[3,2-c]pyridine

There total 3 articles about 2-(N-morpholinyl)-5-(alpha-cyclopropylcarbonyl-2-fluorobenzyl)-4.5.6.7-tetrahydro-thieno-[3,2-c]pyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 204205-33-4
2-bromo-1-cyclopropyl-2-(2-fluorophenyl)ethanone

: 1333429-05-2
2-(4-morpholinyl)-4,5,6,7-tetrahydro-thieno[3,2-c]pyridine

: 1333429-06-3
2-(N-morpholinyl)-5-(alpha-cyclopropylcarbonyl-2-fluorobenzyl)-4.5.6.7-tetrahydro-thieno-[3,2-c]pyridine

Guidance literature:: With triethylamine; In acetonitrile; Cooling with ice;

Reference yield:

: 949922-62-7
2-bromo-6,7-dihydrothieno[3,2-c]pyridine-5(4H)-carboxylic acid tert-butyl ester

: 1333429-06-3
2-(N-morpholinyl)-5-(alpha-cyclopropylcarbonyl-2-fluorobenzyl)-4.5.6.7-tetrahydro-thieno-[3,2-c]pyridine

Guidance literature:: Multi-step reaction with 3 steps

1: potassium phosphate; copper; copper(l) iodide / 2-(N,N-dimethylamino)ethanol / 24 h / 80 °C

2: hydrogenchloride / diethyl ether / Cooling with ice

3: triethylamine / acetonitrile / Cooling with ice

With hydrogenchloride; potassium phosphate; copper(l) iodide; copper; triethylamine; In 2-(N,N-dimethylamino)ethanol; diethyl ether; acetonitrile;

Reference yield:

: 1333429-04-1
2-(4-morpholinyl)-N-tert-butyloxycarbonyl-4,5,6,7-tetrahydro-thieno[3,2-c]pyridine

: 1333429-06-3
2-(N-morpholinyl)-5-(alpha-cyclopropylcarbonyl-2-fluorobenzyl)-4.5.6.7-tetrahydro-thieno-[3,2-c]pyridine

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogenchloride / diethyl ether / Cooling with ice

2: triethylamine / acetonitrile / Cooling with ice

With hydrogenchloride; triethylamine; In diethyl ether; acetonitrile;