2-cyanophenyl dimethylcarbamate

Base Information

Chemical Name:2-cyanophenyl dimethylcarbamate
CAS No.:945-57-3
Molecular Formula:C₁₀H₁₀N₂O₂
Molecular Weight:190.202
Hs Code.:

Synonyms:2-cyanophenyl dimethylcarbamate

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Chemical Property of 2-cyanophenyl dimethylcarbamate

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Technology Process of 2-cyanophenyl dimethylcarbamate

There total 10 articles about 2-cyanophenyl dimethylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 55682-13-8
O-(2-iodophenyl)-N,N-dimethylcarbamate

: 84-58-2
2,3-dicyano-5,6-dichloro-p-benzoquinone

: 945-57-3
2-cyanophenyl dimethylcarbamate

Guidance literature:: With copper diacetate; silver(l) oxide; In 1-methyl-pyrrolidin-2-one; at 120 ℃; for 22h; Sealed tube;
DOI:10.1039/c5cc02533h

Reference yield: 71.0%

: 611-20-1
salicylonitrile

: 68-12-2,33513-42-7
N,N-dimethyl-formamide

: 945-57-3
2-cyanophenyl dimethylcarbamate

Guidance literature:: With di-tert-butyl peroxide; copper 5,10,15,20-tetrakis(ethoxycarbonyl)porphyrin; at 120 ℃; for 12h; Schlenk technique;
DOI:10.1002/jccs.202100046

Reference yield:

: 1360939-08-7
2-deuterio-phenyl dimethylcarbamate

: 945-57-3
2-cyanophenyl dimethylcarbamate

Guidance literature:: Multi-step reaction with 2 steps

1: palladium diacetate; trifluorormethanesulfonic acid; 1-methoxy-1H-1λ³-benzo[d][1,2]iodoxol-3-one / 1,2-dichloro-ethane / 0.5 h / 20 °C / Sealed tube

2: copper diacetate; silver(l) oxide / 1-methyl-pyrrolidin-2-one / 22 h / 120 °C / Sealed tube

With trifluorormethanesulfonic acid; copper diacetate; palladium diacetate; silver(l) oxide; 1-methoxy-1H-1λ³-benzo[d][1,2]iodoxol-3-one; In 1-methyl-pyrrolidin-2-one; 1,2-dichloro-ethane;
DOI:10.1039/c5cc02533h