Technology Process of potassium 3-phenylpropanoyltrifluoroborate
There total 6 articles about potassium 3-phenylpropanoyltrifluoroborate which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
potassium hydrogenfluoride;
In
tetrahydrofuran; water;
at 23 ℃;
for 12h;
DOI:10.1039/c4sc00971a
- Guidance literature:
-
bis(pinacol)diborane;
With
chloro[1,3-bis(2,4,6-trimethylphenyl)imidazol-2-ylidene]copper(I); sodium methylate;
In
tetrahydrofuran;
at 20 ℃;
for 0.166667h;
Inert atmosphere;
Schlenk technique;
4-phenylbutyric acid isobutoxycarbonyl ester;
In
tetrahydrofuran;
at 20 ℃;
for 4h;
Inert atmosphere;
Schlenk technique;
potassium hydrogen difluoride;
In
tetrahydrofuran; water;
at 20 ℃;
for 2h;
Reagent/catalyst;
Temperature;
Catalytic behavior;
Inert atmosphere;
Schlenk technique;
DOI:10.1002/anie.202114513
- Guidance literature:
-
1-(1-phenoxy-4-phenylbutyl)-1H-benzotriazole;
With
n-butyllithium;
In
tetrahydrofuran; hexane;
at -78 ℃;
for 0.0666667h;
Inert atmosphere;
With
Trimethyl borate;
In
tetrahydrofuran; hexane;
at -78 - 20 ℃;
for 1.1h;
Inert atmosphere;
With
potassium hydrogen bifluoride; water;
In
tetrahydrofuran; hexane;
for 14h;
DOI:10.1021/ol300668m
