Technology Process of C30H31F3N4O4
There total 5 articles about C30H31F3N4O4 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: acetic acid / ethanol / 0.25 h / 20 °C
1.2: Reflux
2.1: triethylamine / dmap / tert-butyl alcohol / 16 h / 60 °C
3.1: trichloroisocyanuric acid / 1,1-dichloroethane / 16 h / Reflux
4.1: sodium azide / N,N-dimethyl-formamide / 5 h / 50 °C
5.1: trimethylphosphane / tetrahydrofuran / 3 h / 20 °C
With
sodium azide; trichloroisocyanuric acid; triethylamine; trimethylphosphane;
dmap; acetic acid;
In
tetrahydrofuran; 1,1-dichloroethane; ethanol; N,N-dimethyl-formamide; tert-butyl alcohol;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: triethylamine / dmap / tert-butyl alcohol / 16 h / 60 °C
2: trichloroisocyanuric acid / 1,1-dichloroethane / 16 h / Reflux
3: sodium azide / N,N-dimethyl-formamide / 5 h / 50 °C
4: trimethylphosphane / tetrahydrofuran / 3 h / 20 °C
With
sodium azide; trichloroisocyanuric acid; triethylamine; trimethylphosphane;
dmap;
In
tetrahydrofuran; 1,1-dichloroethane; N,N-dimethyl-formamide; tert-butyl alcohol;
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: ethanol; sodium / 0.5 h / 20 °C
1.2: 16 h / Reflux
2.1: acetic acid / ethanol / 0.25 h / 20 °C
2.2: Reflux
3.1: triethylamine / dmap / tert-butyl alcohol / 16 h / 60 °C
4.1: trichloroisocyanuric acid / 1,1-dichloroethane / 16 h / Reflux
5.1: sodium azide / N,N-dimethyl-formamide / 5 h / 50 °C
6.1: trimethylphosphane / tetrahydrofuran / 3 h / 20 °C
With
sodium azide; ethanol; trichloroisocyanuric acid; sodium; triethylamine; trimethylphosphane;
dmap; acetic acid;
In
tetrahydrofuran; 1,1-dichloroethane; ethanol; N,N-dimethyl-formamide; tert-butyl alcohol;