6-amino-2-ethoxy-4-ferrocenyl-5-ferrocenylmethyl-4,5-dihydropyridine-3,5-dicarbonitrile

Base Information

• Chemical Name: 6-amino-2-ethoxy-4-ferrocenyl-5-ferrocenylmethyl-4,5-dihydropyridine-3,5-dicarbonitrile
• CAS No.: 1416854-27-7
• Molecular Formula: C₃₀H₂₈Fe₂N₄O
• Molecular Weight: 572.273

Synonyms:6-amino-2-ethoxy-4-ferrocenyl-5-ferrocenylmethyl-4,5-dihydropyridine-3,5-dicarbonitrile

Chemical Property of 6-amino-2-ethoxy-4-ferrocenyl-5-ferrocenylmethyl-4,5-dihydropyridine-3,5-dicarbonitrile

Chemical Property:

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Technology Process of 6-amino-2-ethoxy-4-ferrocenyl-5-ferrocenylmethyl-4,5-dihydropyridine-3,5-dicarbonitrile

There total 3 articles about 6-amino-2-ethoxy-4-ferrocenyl-5-ferrocenylmethyl-4,5-dihydropyridine-3,5-dicarbonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 11.0%

2-(ferrocenylmethylidene)malonedinitrile + ethanol (64-17-5) + water (7732-18-5) + benzamidine monohydrochloride (1670-14-0) → ferrocenecarboxaldehyde (12093-10-6) + 6-amino-2-ethoxy-4-ferrocenyl-5-ferrocenylmethyl-4,5-dihydropyridine-3,5-dicarbonitrile (1416854-27-7) + 6-amino-4-ferrocenyl-2-phenyl-3,4-dihydropyrimidine-5-carbonitrile (1416854-30-2) + 2-amino-6-ethoxy-4-ferrocenylpyridine-3,5-dicarbonitrile (1416854-25-5) + 4-amino-6-ferrocenyl-2-phenylpyrimidine-5-carbonitrile (1416854-23-3)

Guidance literature:

With sodium carbonate; at 80 ℃; for 8h;

DOI:10.3987/COM-12-12540

Reference yield: 10.0%

2-(ferrocenylmethylidene)malonedinitrile + ethanol (64-17-5) + water (7732-18-5) + 1,1-dimethylguanidine dihydrogensulfate (311-77-3,1186-46-5) → ferrocenecarboxaldehyde (12093-10-6) + 6-amino-2-ethoxy-4-ferrocenyl-5-ferrocenylmethyl-4,5-dihydropyridine-3,5-dicarbonitrile (1416854-27-7) + 2-amino-6-ethoxy-4-ferrocenylpyridine-3,5-dicarbonitrile (1416854-25-5) + 4-amino-2-dimethylamino-6-ferrocenylpyrimidine-5-carbonitrile (1416854-24-4)

Guidance literature:

With sodium carbonate; at 80 ℃; for 8h;

DOI:10.3987/COM-12-12540

Reference yield: 9.0%

2-(ferrocenylmethylidene)malonedinitrile + ethanol (64-17-5) + water (7732-18-5) + acetamidine hydrochloride (124-42-5) → ferrocenecarboxaldehyde (12093-10-6) + 6-amino-2-ethoxy-4-ferrocenyl-5-ferrocenylmethyl-4,5-dihydropyridine-3,5-dicarbonitrile (1416854-27-7) + 6-amino-4-ferrocenyl-2-methyl-3,4-dihydropyrimidine-5-carbonitrile (1416854-28-8) + 2-amino-6-ethoxy-4-ferrocenylpyridine-3,5-dicarbonitrile (1416854-25-5) + 4-amino-6-ferrocenyl-2-methylpyrimidine-5-carbonitrile (1416854-26-6)

Guidance literature:

With sodium carbonate; at 80 ℃; for 8h;

DOI:10.3987/COM-12-12540

upstream raw materials:

ethanol

water

1,1-dimethylguanidine dihydrogensulfate

acetamidine hydrochloride

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