4-(benzoyl)benzenepropanoic acid N-hydroxysuccinimide ester

Base Information

Chemical Name:4-(benzoyl)benzenepropanoic acid N-hydroxysuccinimide ester
CAS No.:161364-95-0
Molecular Formula:C₂₀H₁₇NO₅
Molecular Weight:351.359
Hs Code.:

Synonyms:4-(benzoyl)benzenepropanoic acid N-hydroxysuccinimide ester

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Chemical Property of 4-(benzoyl)benzenepropanoic acid N-hydroxysuccinimide ester

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Technology Process of 4-(benzoyl)benzenepropanoic acid N-hydroxysuccinimide ester

There total 4 articles about 4-(benzoyl)benzenepropanoic acid N-hydroxysuccinimide ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 6136-66-9
4-iodobenzophenone

: 161364-95-0
4-(benzoyl)benzenepropanoic acid N-hydroxysuccinimide ester

Guidance literature:: Multi-step reaction with 4 steps

1: 85 percent / Bu₄NCl; NaHCO₃ / Pd(OAc)2 / dimethylformamide / 3 h / 20 °C

2: 95 percent / H₂ / PtO₂ / ethyl acetate / 0.08 h / 20 °C

3: 100 percent / NaOH / dioxane; H₂O / 2 h / 20 °C

4: DCC / CH₂Cl₂

With sodium hydroxide; tetrabutyl-ammonium chloride; hydrogen; sodium hydrogencarbonate; dicyclohexyl-carbodiimide; platinum(IV) oxide; palladium diacetate; In 1,4-dioxane; dichloromethane; water; ethyl acetate; N,N-dimethyl-formamide; 1: Heck coupling / 2: Catalytic hydrogenation / 3: Hydrolysis / 4: Substitution;
DOI:10.1002/1099-0690(200009)2000:17<3085::AID-EJOC3085>3.0.CO;2-A

Reference yield:

: 305839-17-2
methyl (E)?3?(4?benzoylphenyl)acrylate

: 161364-95-0
4-(benzoyl)benzenepropanoic acid N-hydroxysuccinimide ester

Guidance literature:: Multi-step reaction with 3 steps

1: 95 percent / H₂ / PtO₂ / ethyl acetate / 0.08 h / 20 °C

2: 100 percent / NaOH / dioxane; H₂O / 2 h / 20 °C

3: DCC / CH₂Cl₂

With sodium hydroxide; hydrogen; dicyclohexyl-carbodiimide; platinum(IV) oxide; In 1,4-dioxane; dichloromethane; water; ethyl acetate; 1: Catalytic hydrogenation / 2: Hydrolysis / 3: Substitution;
DOI:10.1002/1099-0690(200009)2000:17<3085::AID-EJOC3085>3.0.CO;2-A

Reference yield:

: 305839-15-0
methyl p-benzoyl-2,3-didehydrocinnamate

: 161364-95-0
4-(benzoyl)benzenepropanoic acid N-hydroxysuccinimide ester

Guidance literature:: Multi-step reaction with 3 steps

1: 95 percent / H₂ / PtO₂ / ethyl acetate / 0.08 h / 20 °C

2: 100 percent / NaOH / dioxane; H₂O / 2 h / 20 °C

3: DCC / CH₂Cl₂

With sodium hydroxide; hydrogen; dicyclohexyl-carbodiimide; platinum(IV) oxide; In 1,4-dioxane; dichloromethane; water; ethyl acetate; 1: Catalytic hydrogenation / 2: Hydrolysis / 3: Substitution;
DOI:10.1002/1099-0690(200009)2000:17<3085::AID-EJOC3085>3.0.CO;2-A