dimethyl (((4-methylphenyl)sulfonamido)(thiophen-2-yl)methyl)phosphonate

Base Information

Chemical Name:dimethyl (((4-methylphenyl)sulfonamido)(thiophen-2-yl)methyl)phosphonate
CAS No.:1154063-27-0
Molecular Formula:C₁₄H₁₈NO₅PS₂
Molecular Weight:375.406
Hs Code.:

Synonyms:dimethyl (((4-methylphenyl)sulfonamido)(thiophen-2-yl)methyl)phosphonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of dimethyl (((4-methylphenyl)sulfonamido)(thiophen-2-yl)methyl)phosphonate

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Technology Process of dimethyl (((4-methylphenyl)sulfonamido)(thiophen-2-yl)methyl)phosphonate

There total 4 articles about dimethyl (((4-methylphenyl)sulfonamido)(thiophen-2-yl)methyl)phosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 36198-87-5
dimethyl trimethylsilyl phosphite

: 158293-42-6
4-methyl-N-(thiophen-2-ylmethylene)benzenesulfonamide

: 1154063-27-0
dimethyl (((4-methylphenyl)sulfonamido)(thiophen-2-yl)methyl)phosphonate

Guidance literature:: With Amberlyst-15; In dichloromethane; at 0 ℃; for 2.5h; Inert atmosphere;
DOI:10.1080/00397911003707188

Reference yield: 88.0%

: 96-36-6,868-85-9
methyl phosphite

: 158293-42-6
4-methyl-N-(thiophen-2-ylmethylene)benzenesulfonamide

: 1154063-27-0
dimethyl (((4-methylphenyl)sulfonamido)(thiophen-2-yl)methyl)phosphonate

Guidance literature:: With triethylamine; In toluene; for 24h; Reflux; Inert atmosphere;
DOI:10.1021/acs.orglett.9b03669

Reference yield:

: 98-03-3
thiophene-2-carbaldehyde

: 70-55-3
toluene-4-sulfonamide

: 868-85-9
Dimethyl phosphite

: 1154063-27-0
dimethyl (((4-methylphenyl)sulfonamido)(thiophen-2-yl)methyl)phosphonate

Guidance literature:: With magnesium(II) perchlorate; In neat (no solvent); at 150 ℃; for 0.0833333h; chemoselective reaction; Microwave irradiation; Green chemistry;
DOI:10.1016/j.bioorg.2018.09.023