3-{4-[(4-{[(2Z)-2-(methoxyimino)-2-phenylethyl]oxy}benzyl)oxy]phenyl}propanamide

Base Information

Chemical Name:3-{4-[(4-{[(2Z)-2-(methoxyimino)-2-phenylethyl]oxy}benzyl)oxy]phenyl}propanamide
CAS No.:1356599-75-1
Molecular Formula:C₂₅H₂₆N₂O₄
Molecular Weight:418.492
Hs Code.:

Synonyms:3-{4-[(4-{[(2Z)-2-(methoxyimino)-2-phenylethyl]oxy}benzyl)oxy]phenyl}propanamide

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Chemical Property of 3-{4-[(4-{[(2Z)-2-(methoxyimino)-2-phenylethyl]oxy}benzyl)oxy]phenyl}propanamide

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Technology Process of 3-{4-[(4-{[(2Z)-2-(methoxyimino)-2-phenylethyl]oxy}benzyl)oxy]phenyl}propanamide

There total 7 articles about 3-{4-[(4-{[(2Z)-2-(methoxyimino)-2-phenylethyl]oxy}benzyl)oxy]phenyl}propanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5597-50-2
3-(4-hydroxyphenyl)propionic acid methyl ester

: 1356599-75-1
3-{4-[(4-{[(2Z)-2-(methoxyimino)-2-phenylethyl]oxy}benzyl)oxy]phenyl}propanamide

Guidance literature:: Multi-step reaction with 4 steps

1.1: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 0 - 20 °C

2.1: sodium hydroxide; water / tetrahydrofuran; methanol / 12 h / 20 °C

2.2: 20 °C

3.1: chloroformic acid ethyl ester; triethylamine / tetrahydrofuran / 0.75 h / -10 °C

3.2: 1 h / -10 °C

4.1: sodium acetate; acetic acid / 12 h / 20 °C

4.2: 20 °C

With di-isopropyl azodicarboxylate; water; sodium acetate; chloroformic acid ethyl ester; acetic acid; triethylamine; triphenylphosphine; sodium hydroxide; In tetrahydrofuran; methanol;

Reference yield:

: 1356602-65-7
3-(4-{[4-(2-oxo-2-phenylethoxy)benzyl]oxy}phenyl)propanamide

: 593-56-6
N-methoxylamine hydrochloride

: 1356599-75-1
3-{4-[(4-{[(2Z)-2-(methoxyimino)-2-phenylethyl]oxy}benzyl)oxy]phenyl}propanamide

Guidance literature:: 3-(4-{[4-(2-oxo-2-phenylethoxy)benzyl]oxy}phenyl)propanamide; N-methoxylamine hydrochloride; With sodium acetate; acetic acid; at 20 ℃; for 12h;

With sodium carbonate; at 20 ℃;

Reference yield:

: 70-11-1
α-bromoacetophenone

: 1356599-75-1
3-{4-[(4-{[(2Z)-2-(methoxyimino)-2-phenylethyl]oxy}benzyl)oxy]phenyl}propanamide

Guidance literature:: Multi-step reaction with 5 steps

1.1: potassium carbonate / acetonitrile / 2 h / 20 - 80 °C

2.1: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 0 - 20 °C

3.1: sodium hydroxide; water / tetrahydrofuran; methanol / 12 h / 20 °C

3.2: 20 °C

4.1: chloroformic acid ethyl ester; triethylamine / tetrahydrofuran / 0.75 h / -10 °C

4.2: 1 h / -10 °C

5.1: sodium acetate; acetic acid / 12 h / 20 °C

5.2: 20 °C

With di-isopropyl azodicarboxylate; water; sodium acetate; chloroformic acid ethyl ester; potassium carbonate; acetic acid; triethylamine; triphenylphosphine; sodium hydroxide; In tetrahydrofuran; methanol; acetonitrile;