2-Methoxy-4-(phenylmethyl)-3-pyridinecarbamic acid 1,1-dimethylethyl ester

Base Information

Chemical Name:2-Methoxy-4-(phenylmethyl)-3-pyridinecarbamic acid 1,1-dimethylethyl ester
CAS No.:162709-18-4
Molecular Formula:C₁₈H₂₂N₂O₃
Molecular Weight:314.384
Hs Code.:

Synonyms:2-Methoxy-4-(phenylmethyl)-3-pyridinecarbamic acid 1,1-dimethylethyl ester

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Chemical Property of 2-Methoxy-4-(phenylmethyl)-3-pyridinecarbamic acid 1,1-dimethylethyl ester

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Technology Process of 2-Methoxy-4-(phenylmethyl)-3-pyridinecarbamic acid 1,1-dimethylethyl ester

There total 1 articles about 2-Methoxy-4-(phenylmethyl)-3-pyridinecarbamic acid 1,1-dimethylethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 100-39-0
benzyl bromide

: 161117-83-5
3-(N-tert-butoxycarbonylamino)-2-methoxypyridine

: 162709-18-4
2-Methoxy-4-(phenylmethyl)-3-pyridinecarbamic acid 1,1-dimethylethyl ester

Guidance literature:: With n-butyllithium; N,N,N,N,-tetramethylethylenediamine; In diethyl ether; hexane; 1.) -78 to -10 deg C, 2 h, 2.) -78 deg C to r.t., 3 h;
DOI:10.1021/jo00111a056

Reference yield: 99.0%

: 162709-18-4
2-Methoxy-4-(phenylmethyl)-3-pyridinecarbamic acid 1,1-dimethylethyl ester

: 3-amino-2-methoxy-4-(phenylmethyl)pyridine

Guidance literature:: With hydrogenchloride; In ethyl acetate;
DOI:10.1021/jm00024a011

Reference yield:

: 162709-18-4
2-Methoxy-4-(phenylmethyl)-3-pyridinecarbamic acid 1,1-dimethylethyl ester

: 2-chloro-N-<2-methoxy-4-(phenylmethyl)-3-pyridinyl>-3-pyridinecarboxamide

Guidance literature:: Multi-step reaction with 2 steps

1: 99 percent / HCl / ethyl acetate

2: 77 percent / i-PrNEt₂ / ethyl acetate / 0 °C

With hydrogenchloride; N,N-diethyl-N-isopropylamine; In ethyl acetate;
DOI:10.1021/jm00024a011