(2S,4S)-1-(tert-butoxycarbonyl)-5-oxo-4-phenylaminoproline methyl ester

Base Information

Chemical Name:(2S,4S)-1-(tert-butoxycarbonyl)-5-oxo-4-phenylaminoproline methyl ester
CAS No.:1350477-09-6
Molecular Formula:C₁₇H₂₂N₂O₅
Molecular Weight:334.372
Hs Code.:

Synonyms:(2S,4S)-1-(tert-butoxycarbonyl)-5-oxo-4-phenylaminoproline methyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2S,4S)-1-(tert-butoxycarbonyl)-5-oxo-4-phenylaminoproline methyl ester

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Technology Process of (2S,4S)-1-(tert-butoxycarbonyl)-5-oxo-4-phenylaminoproline methyl ester

There total 1 articles about (2S,4S)-1-(tert-butoxycarbonyl)-5-oxo-4-phenylaminoproline methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 1032764-56-9
methyl (2S,4S)-5-oxo-4-phenylaminoprolinate

: 24424-99-5
di-tert-butyl dicarbonate

: 1350477-09-6
(2S,4S)-1-(tert-butoxycarbonyl)-5-oxo-4-phenylaminoproline methyl ester

Guidance literature:: With dmap; triethylamine; In dichloromethane; at 20 ℃; for 2h;
DOI:10.1007/s11172-011-0137-4

Reference yield: 72.0%

: 1350477-09-6
(2S,4S)-1-(tert-butoxycarbonyl)-5-oxo-4-phenylaminoproline methyl ester

: 1350477-15-4
2-(tert-butoxycarbonyl)-5-phenyl-2,5-diazabicyclo[2.2.1]heptane

: 1350477-13-2
(2S,4S)-1-(tert-butoxycarbonyl)-2-hydroxymethyl-4-phenylaminopyrrolidine

Guidance literature:: With borane dimethyl sulphide complex; In tetrahydrofuran; at 40 ℃; for 96h; Inert atmosphere;
DOI:10.1007/s11172-011-0137-4

Reference yield: 63.0%

: 1350477-09-6
(2S,4S)-1-(tert-butoxycarbonyl)-5-oxo-4-phenylaminoproline methyl ester

: 1350477-11-0
(2S,4S)-1-(tert-butoxycarbonyl)-4-phenylaminoproline methyl ester

Guidance literature:: With borane dimethyl sulphide complex; In tetrahydrofuran; at -5 ℃; for 408h; Inert atmosphere;
DOI:10.1007/s11172-011-0137-4