C₉H₇ClF₃IO

Base Information

• Chemical Name: C₉H₇ClF₃IO
• CAS No.: 1259539-26-8
• Molecular Formula: C₉H₇ClF₃IO
• Molecular Weight: 350.507
• Mol file: 1259539-26-8.mol

Synonyms:C₉H₇ClF₃IO

Chemical Property of C₉H₇ClF₃IO

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of C₉H₇ClF₃IO

There total 1 articles about C₉H₇ClF₃IO which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

C9H9ClF3NO (1259539-25-7) → C9H7ClF3IO (1259539-26-8)

Guidance literature:

C₉H₉ClF₃NO; With hydrogenchloride; sodium nitrite; for 0.5h; Cooling;

With potassium iodide; at 20 ℃; for 8h;

DOI:10.1016/j.bmcl.2010.10.012

Reference yield: 98.0%

methanol (67-56-1) + carbon monoxide (201230-82-2) + C9H7ClF3IO (1259539-26-8) → C11H10ClF3O3 (1259539-28-0)

Guidance literature:

With palladium diacetate; triethylamine; In N,N-dimethyl-formamide; at 50 ℃; for 6h; under 4500.45 Torr;

DOI:10.1016/j.bmcl.2010.10.012

upstream raw materials:

C₉H₉ClF₃NO

Downstream raw materials:

C₁₁H₁₀ClF₃O₃