phenylmethyl (7-iodo-5-phenyl-2-thioxo-2,3-dihydro-1H-1,4-benzo diazepin-3-yl)carbamate

Base Information

Chemical Name:phenylmethyl (7-iodo-5-phenyl-2-thioxo-2,3-dihydro-1H-1,4-benzo diazepin-3-yl)carbamate
CAS No.:1300089-84-2
Molecular Formula:C₂₃H₁₈IN₃O₂S
Molecular Weight:527.385
Hs Code.:

Synonyms:phenylmethyl (7-iodo-5-phenyl-2-thioxo-2,3-dihydro-1H-1,4-benzo diazepin-3-yl)carbamate

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Chemical Property of phenylmethyl (7-iodo-5-phenyl-2-thioxo-2,3-dihydro-1H-1,4-benzo diazepin-3-yl)carbamate

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Technology Process of phenylmethyl (7-iodo-5-phenyl-2-thioxo-2,3-dihydro-1H-1,4-benzo diazepin-3-yl)carbamate

There total 6 articles about phenylmethyl (7-iodo-5-phenyl-2-thioxo-2,3-dihydro-1H-1,4-benzo diazepin-3-yl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1300090-04-3
benzyl N-(7-iodo-2-oxo-5-phenyl-2,3-dihydro-1H-1,4-benzodiazepin-3-yl)carbamate

: 1300089-84-2
phenylmethyl (7-iodo-5-phenyl-2-thioxo-2,3-dihydro-1H-1,4-benzo diazepin-3-yl)carbamate

Guidance literature:: With Lawessons reagent; In toluene; at 100 ℃; for 3h;

Reference yield:

: 2835-77-0
(2-aminophenyl)(phenyl)methanone

: 1300089-84-2
phenylmethyl (7-iodo-5-phenyl-2-thioxo-2,3-dihydro-1H-1,4-benzo diazepin-3-yl)carbamate

Guidance literature:: Multi-step reaction with 4 steps

1.1: Iodine monochloride / dichloromethane / -70 - 20 °C

2.1: N,N-dimethyl-formamide; oxalyl dichloride / tetrahydrofuran / 3 h / 0 °C

2.2: 0 - 20 °C

2.3: 1 h / 0 °C

3.1: ammonium acetate; acetic acid / 3 h / 20 °C

4.1: Lawessons reagent / toluene / 3 h / 100 °C

With Lawessons reagent; oxalyl dichloride; ammonium acetate; Iodine monochloride; acetic acid; N,N-dimethyl-formamide; In tetrahydrofuran; dichloromethane; toluene;

Reference yield:

: 51073-69-9
(2-amino-5-iodophenyl)(phenyl)methanone

: 1300089-84-2
phenylmethyl (7-iodo-5-phenyl-2-thioxo-2,3-dihydro-1H-1,4-benzo diazepin-3-yl)carbamate

Guidance literature:: Multi-step reaction with 3 steps

1.1: N,N-dimethyl-formamide; oxalyl dichloride / tetrahydrofuran / 3 h / 0 °C

1.2: 0 - 20 °C

1.3: 1 h / 0 °C

2.1: ammonium acetate; acetic acid / 3 h / 20 °C

3.1: Lawessons reagent / toluene / 3 h / 100 °C

With Lawessons reagent; oxalyl dichloride; ammonium acetate; acetic acid; N,N-dimethyl-formamide; In tetrahydrofuran; toluene;