5-(2-(benzyloxy)-2-oxoethyl)-2-((3,5-dimethylisoxazol-4-yl)methoxy)benzoic acid

Base Information

Chemical Name:5-(2-(benzyloxy)-2-oxoethyl)-2-((3,5-dimethylisoxazol-4-yl)methoxy)benzoic acid
CAS No.:1421838-34-7
Molecular Formula:C₂₂H₂₁NO₆
Molecular Weight:395.412
Hs Code.:

Synonyms:5-(2-(benzyloxy)-2-oxoethyl)-2-((3,5-dimethylisoxazol-4-yl)methoxy)benzoic acid

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Chemical Property of 5-(2-(benzyloxy)-2-oxoethyl)-2-((3,5-dimethylisoxazol-4-yl)methoxy)benzoic acid

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Technology Process of 5-(2-(benzyloxy)-2-oxoethyl)-2-((3,5-dimethylisoxazol-4-yl)methoxy)benzoic acid

There total 5 articles about 5-(2-(benzyloxy)-2-oxoethyl)-2-((3,5-dimethylisoxazol-4-yl)methoxy)benzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.8%

: 1421838-33-6
benzyl 2-(4-((3,5-dimethylisoxazol-4-yl)metoxy)-3-formylphenyl)acetate

: 1421838-34-7
5-(2-(benzyloxy)-2-oxoethyl)-2-((3,5-dimethylisoxazol-4-yl)methoxy)benzoic acid

Guidance literature:: With sodium chlorite; sodium dihydrogenphosphate; In water; dimethyl sulfoxide; at 20 ℃;

Reference yield:

: 100-39-0
benzyl bromide

: 1421838-34-7
5-(2-(benzyloxy)-2-oxoethyl)-2-((3,5-dimethylisoxazol-4-yl)methoxy)benzoic acid

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium hydride / N,N-dimethyl-formamide / 0.5 h / 0 °C

1.2: 1 h

2.1: triethylamine; magnesium chloride / acetonitrile / 1 h / Reflux; Inert atmosphere

2.2: Reflux

3.1: potassium carbonate; potassium iodide / acetonitrile / Reflux

4.1: sodium dihydrogenphosphate; sodium chlorite / water; dimethyl sulfoxide / 20 °C

With sodium chlorite; sodium dihydrogenphosphate; sodium hydride; potassium carbonate; triethylamine; potassium iodide; magnesium chloride; In water; dimethyl sulfoxide; N,N-dimethyl-formamide; acetonitrile;

Reference yield:

: 1421838-32-5
benzyl 2-(3-formyl-4-hydroxyphenyl)acetate

: 1421838-34-7
5-(2-(benzyloxy)-2-oxoethyl)-2-((3,5-dimethylisoxazol-4-yl)methoxy)benzoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate; potassium iodide / acetonitrile / Reflux

2: sodium dihydrogenphosphate; sodium chlorite / water; dimethyl sulfoxide / 20 °C

With sodium chlorite; sodium dihydrogenphosphate; potassium carbonate; potassium iodide; In water; dimethyl sulfoxide; acetonitrile;