methyl 5-(2-(benzyloxy)-2-oxoethyl)-2-((3,5-dimethylisoxazol-4-yl)methoxy)benzoate

Base Information

Chemical Name:methyl 5-(2-(benzyloxy)-2-oxoethyl)-2-((3,5-dimethylisoxazol-4-yl)methoxy)benzoate
CAS No.:1421838-35-8
Molecular Formula:C₂₃H₂₃NO₆
Molecular Weight:409.439
Hs Code.:

Synonyms:methyl 5-(2-(benzyloxy)-2-oxoethyl)-2-((3,5-dimethylisoxazol-4-yl)methoxy)benzoate

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Chemical Property of methyl 5-(2-(benzyloxy)-2-oxoethyl)-2-((3,5-dimethylisoxazol-4-yl)methoxy)benzoate

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Technology Process of methyl 5-(2-(benzyloxy)-2-oxoethyl)-2-((3,5-dimethylisoxazol-4-yl)methoxy)benzoate

There total 6 articles about methyl 5-(2-(benzyloxy)-2-oxoethyl)-2-((3,5-dimethylisoxazol-4-yl)methoxy)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.7%

: 1421838-34-7
5-(2-(benzyloxy)-2-oxoethyl)-2-((3,5-dimethylisoxazol-4-yl)methoxy)benzoic acid

: 74-88-4
methyl iodide

: 1421838-35-8
methyl 5-(2-(benzyloxy)-2-oxoethyl)-2-((3,5-dimethylisoxazol-4-yl)methoxy)benzoate

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃;

Reference yield:

: 100-39-0
benzyl bromide

: 1421838-35-8
methyl 5-(2-(benzyloxy)-2-oxoethyl)-2-((3,5-dimethylisoxazol-4-yl)methoxy)benzoate

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium hydride / N,N-dimethyl-formamide / 0.5 h / 0 °C

1.2: 1 h

2.1: triethylamine; magnesium chloride / acetonitrile / 1 h / Reflux; Inert atmosphere

2.2: Reflux

3.1: potassium carbonate; potassium iodide / acetonitrile / Reflux

4.1: sodium dihydrogenphosphate; sodium chlorite / water; dimethyl sulfoxide / 20 °C

5.1: potassium carbonate / N,N-dimethyl-formamide / 20 °C

With sodium chlorite; sodium dihydrogenphosphate; sodium hydride; potassium carbonate; triethylamine; potassium iodide; magnesium chloride; In water; dimethyl sulfoxide; N,N-dimethyl-formamide; acetonitrile;

Reference yield:

: 156-38-7
4-hydroxyphenylacetate

: 1421838-35-8
methyl 5-(2-(benzyloxy)-2-oxoethyl)-2-((3,5-dimethylisoxazol-4-yl)methoxy)benzoate

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium hydride / N,N-dimethyl-formamide / 0.5 h / 0 °C

1.2: 1 h

2.1: triethylamine; magnesium chloride / acetonitrile / 1 h / Reflux; Inert atmosphere

2.2: Reflux

3.1: potassium carbonate; potassium iodide / acetonitrile / Reflux

4.1: sodium dihydrogenphosphate; sodium chlorite / water; dimethyl sulfoxide / 20 °C

5.1: potassium carbonate / N,N-dimethyl-formamide / 20 °C

With sodium chlorite; sodium dihydrogenphosphate; sodium hydride; potassium carbonate; triethylamine; potassium iodide; magnesium chloride; In water; dimethyl sulfoxide; N,N-dimethyl-formamide; acetonitrile;