trimethyl({3,3,6,6-tetramethyl-2-[(trimethylsilyl)oxy]cyclohex-1-en-1-yl}oxy)silane

Base Information

Chemical Name:trimethyl({3,3,6,6-tetramethyl-2-[(trimethylsilyl)oxy]cyclohex-1-en-1-yl}oxy)silane
CAS No.:177263-27-3
Molecular Formula:C₁₆H₃₄O₂Si₂
Molecular Weight:314.616
Hs Code.:

Synonyms:trimethyl({3,3,6,6-tetramethyl-2-[(trimethylsilyl)oxy]cyclohex-1-en-1-yl}oxy)silane

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Chemical Property of trimethyl({3,3,6,6-tetramethyl-2-[(trimethylsilyl)oxy]cyclohex-1-en-1-yl}oxy)silane

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Technology Process of trimethyl({3,3,6,6-tetramethyl-2-[(trimethylsilyl)oxy]cyclohex-1-en-1-yl}oxy)silane

There total 4 articles about trimethyl({3,3,6,6-tetramethyl-2-[(trimethylsilyl)oxy]cyclohex-1-en-1-yl}oxy)silane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 75-77-4
chloro-trimethyl-silane

: 5238-36-8
1,6-diethyl 2,2,5,5-tetramethylhexanedioate

: 177263-27-3
trimethyl({3,3,6,6-tetramethyl-2-[(trimethylsilyl)oxy]cyclohex-1-en-1-yl}oxy)silane

Guidance literature:: With sodium; In toluene; Inert atmosphere; Reflux;

Reference yield: 6.0%

: 75-77-4
chloro-trimethyl-silane

: 20651-89-2
3,3,6,6-tetramethylcyclohexane-1,2-dione

: 177263-27-3
trimethyl({3,3,6,6-tetramethyl-2-[(trimethylsilyl)oxy]cyclohex-1-en-1-yl}oxy)silane

Guidance literature:: With sodium; In 1,2-dimethoxyethane; for 14h;

Reference yield:

: 4916-85-2
2,2,5,5-tetramethylhexanedioic acid

: 177263-27-3
trimethyl({3,3,6,6-tetramethyl-2-[(trimethylsilyl)oxy]cyclohex-1-en-1-yl}oxy)silane

Guidance literature:: Multi-step reaction with 2 steps

1: 83.2 percent / conc. H₂SO₄ / benzene / 12 h / Heating

2: 72 percent / Na / toluene / 20 h / 90 °C

With sulfuric acid; sodium; In toluene; benzene;
DOI:10.1021/jm9801354