1-phenylethyl mesylate

Base Information

Chemical Name:1-phenylethyl mesylate
CAS No.:25236-63-9
Molecular Formula:C₉H₁₂O₃S
Molecular Weight:200.258
Hs Code.:

Synonyms:1-phenylethyl mesylate

Suppliers and Price of 1-phenylethyl mesylate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-phenylethyl mesylate

Chemical Property:

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Technology Process of 1-phenylethyl mesylate

There total 2 articles about 1-phenylethyl mesylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 98-85-1,13323-81-4
1-Phenylethanol

: 124-63-0
methanesulfonyl chloride

: 25236-63-9
1-phenylethyl mesylate

Guidance literature:: With triethylamine; In dichloromethane;
DOI:10.1021/jo00834a087

Reference yield:

: 98-86-2
acetophenone

: 25236-63-9
1-phenylethyl mesylate

Guidance literature:: Multi-step reaction with 2 steps

1: sodium tetrahydroborate; methanol / 1 h / Cooling with ice

2: triethylamine / dichloromethane / 12 h / Cooling with ice

With methanol; sodium tetrahydroborate; triethylamine; In dichloromethane;
DOI:10.1016/j.bmc.2018.04.041

Reference yield: 60.0%

: 5798-75-4
Ethyl 4-bromobenzoate

: 25236-63-9
1-phenylethyl mesylate

: 1048028-22-3
4-(1-phenylethyl)benzoic acid ethyl ester

Guidance literature:: Ethyl 4-bromobenzoate; 1-phenylethyl mesylate; With manganese; trifluoroacetic acid; In acetonitrile; for 0.166667h;

With cobalt(II) bromide; In acetonitrile; at 45 ℃; for 2h;
DOI:10.1002/adsc.201800468