(7R)-10,10-diethyl-2,2,7-trimethyl-8-((S)-3-methylhex-5-enyl)-3,3-diphenyl-4,9-dioxa-3,10-disiladodecane

Base Information

Chemical Name:(7R)-10,10-diethyl-2,2,7-trimethyl-8-((S)-3-methylhex-5-enyl)-3,3-diphenyl-4,9-dioxa-3,10-disiladodecane
CAS No.:1255910-53-2
Molecular Formula:C₃₄H₅₆O₂Si₂
Molecular Weight:552.988
Hs Code.:

Synonyms:(7R)-10,10-diethyl-2,2,7-trimethyl-8-((S)-3-methylhex-5-enyl)-3,3-diphenyl-4,9-dioxa-3,10-disiladodecane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (7R)-10,10-diethyl-2,2,7-trimethyl-8-((S)-3-methylhex-5-enyl)-3,3-diphenyl-4,9-dioxa-3,10-disiladodecane

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Technology Process of (7R)-10,10-diethyl-2,2,7-trimethyl-8-((S)-3-methylhex-5-enyl)-3,3-diphenyl-4,9-dioxa-3,10-disiladodecane

There total 1 articles about (7R)-10,10-diethyl-2,2,7-trimethyl-8-((S)-3-methylhex-5-enyl)-3,3-diphenyl-4,9-dioxa-3,10-disiladodecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 1255910-60-1
(3S,7R)-9-(tert-butyldiphenylsilyloxy)-3,7-dimethyl-6-(triethylsilyloxy)nonan-1-ol

: 1779-49-3
Methyltriphenylphosphonium bromide

: 1255910-53-2
(7R)-10,10-diethyl-2,2,7-trimethyl-8-((S)-3-methylhex-5-enyl)-3,3-diphenyl-4,9-dioxa-3,10-disiladodecane

Guidance literature:: (3S,7R)-9-(tert-butyldiphenylsilyloxy)-3,7-dimethyl-6-(triethylsilyloxy)nonan-1-ol; With sodium hydrogencarbonate; Dess-Martin periodane; In dichloromethane; at 20 ℃; for 1h; Inert atmosphere;

Methyltriphenylphosphonium bromide; With lithium hexamethyldisilazane; In tetrahydrofuran; at 0 ℃; Inert atmosphere;
DOI:10.1021/ol102177j

Reference yield: 60.0%

: 1255910-55-4
(3S,7R)-8-(tert-butyldiphenylsilyloxy)-3,7-dimethyloct-1-en-3-ol

: 1255910-53-2
(7R)-10,10-diethyl-2,2,7-trimethyl-8-((S)-3-methylhex-5-enyl)-3,3-diphenyl-4,9-dioxa-3,10-disiladodecane

: 1255910-72-5
(6R,10S,14S,18R)-2,2,6,10,14,18,23,23-octamethyl-3,3,22,22-tetraphenyl-17-(triethylsilyloxy)-4,21-dioxa-3,22-disilatetracos-11-en-10-ol

Guidance literature:: With Hoveyda-Grubbs catalyst second generation; In α,α,α-trifluorotoluene; at 85 ℃; for 2h; Inert atmosphere;
DOI:10.1021/ol102177j