methyl dl-1,2,3,4-tetrahydro-9H-pyrido<3,4-b>indole-2-(4-chlorobenzoyl)-3-carboxylate

Base Information

Chemical Name:methyl dl-1,2,3,4-tetrahydro-9H-pyrido<3,4-b>indole-2-(4-chlorobenzoyl)-3-carboxylate
CAS No.:125094-50-0
Molecular Formula:C₂₀H₁₇ClN₂O₃
Molecular Weight:368.82
Hs Code.:

Synonyms:methyl dl-1,2,3,4-tetrahydro-9H-pyrido<3,4-b>indole-2-(4-chlorobenzoyl)-3-carboxylate

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Chemical Property of methyl dl-1,2,3,4-tetrahydro-9H-pyrido<3,4-b>indole-2-(4-chlorobenzoyl)-3-carboxylate

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Technology Process of methyl dl-1,2,3,4-tetrahydro-9H-pyrido<3,4-b>indole-2-(4-chlorobenzoyl)-3-carboxylate

There total 3 articles about methyl dl-1,2,3,4-tetrahydro-9H-pyrido<3,4-b>indole-2-(4-chlorobenzoyl)-3-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 98-88-4
benzoyl chloride

: 42021-11-4
methyl 1,2,3,4-tetrahydro-β-carboline-3-carboxylate

: 125094-50-0
methyl dl-1,2,3,4-tetrahydro-9H-pyrido<3,4-b>indole-2-(4-chlorobenzoyl)-3-carboxylate

Guidance literature:: With triethylamine; In tetrahydrofuran; for 9h; Reflux;

Reference yield: 52.0%

: 122-01-0
4-chloro-benzoyl chloride

: 42021-11-4
methyl 1,2,3,4-tetrahydro-β-carboline-3-carboxylate

: 125094-50-0
methyl dl-1,2,3,4-tetrahydro-9H-pyrido<3,4-b>indole-2-(4-chlorobenzoyl)-3-carboxylate

Guidance literature:: With triethylamine; In tetrahydrofuran; for 16h; Heating;

Reference yield:

: 4299-70-1
L-tryptophan methyl ester

: 125094-50-0
methyl dl-1,2,3,4-tetrahydro-9H-pyrido<3,4-b>indole-2-(4-chlorobenzoyl)-3-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: methanol / water / 5 h / 20 °C

2: triethylamine / tetrahydrofuran / 9 h / Reflux

With methanol; triethylamine; In tetrahydrofuran; water;