phenyl 10-methyl-10λ⁴-acridine-9-carboxylate trifluoromethanesulfonate

Base Information

• Chemical Name: phenyl 10-methyl-10λ⁴-acridine-9-carboxylate trifluoromethanesulfonate
• CAS No.: 161006-14-0
• Molecular Formula: CF₃O₃S*C₂₁H₁₆NO₂
• Molecular Weight: 463.434

Synonyms:phenyl 10-methyl-10λ⁴-acridine-9-carboxylate trifluoromethanesulfonate

Chemical Property of phenyl 10-methyl-10λ⁴-acridine-9-carboxylate trifluoromethanesulfonate

Chemical Property:

• Melting Point: 228-230 °C

Purity/Quality:

98% ^*data from raw suppliers

10-methyl-9-(phenoxycarbonyl) Acridinium (trifluoromethylsulfonate) ≥95% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Description: 10-methyl-9-(phenoxycarbonyl) Acridinium is an acridinium ester that produces fluorescent 10-methyl-9-acridone upon oxidation with hydrogen peroxide, persulfates, and other oxidants in alkaline conditions. Acridinium salts, including 10-methyl-9-(phenoxycarbonyl) acridinium, can be used in chemiluminescence assays, enzyme, antigen, antibody, and hormone immunoassays, and assays to detect oxidants in environmental, biological, and pharmaceutical samples.

Technology Process of phenyl 10-methyl-10λ⁴-acridine-9-carboxylate trifluoromethanesulfonate

There total 5 articles about phenyl 10-methyl-10λ⁴-acridine-9-carboxylate trifluoromethanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

phenyl acridine-9-carboxylate (109392-90-7) + methyl trifluoromethanesulfonate (333-27-7) → phenyl 10-methyl-10λ4-acridine-9-carboxylate trifluoromethanesulfonate (161006-14-0)

Guidance literature:

In dichloromethane; at 20 ℃;

DOI:10.1016/j.saa.2007.10.045

Reference yield:

phenyl acridine-9-carboxylate (109392-90-7) → phenyl 10-methyl-10λ4-acridine-9-carboxylate trifluoromethanesulfonate (161006-14-0)

Guidance literature:

In dichloromethane;

Reference yield:

acridine-9-carboxylic acid (5336-90-3) → phenyl 10-methyl-10λ4-acridine-9-carboxylate trifluoromethanesulfonate (161006-14-0)

Guidance literature:

Multi-step reaction with 3 steps

1: thionyl chloride / Reflux

2: dmap; triethylamine / dichloromethane / 20 °C

3: dichloromethane / 20 °C / Inert atmosphere

With dmap; thionyl chloride; triethylamine; In dichloromethane;

DOI:10.1021/jo1020882

upstream raw materials:

phenyl acridine-9-carboxylate

methyl trifluoromethanesulfonate

acridine-9-carboxylic acid

9-acridinecarbonyl chloride

Downstream raw materials:

10-methyl-9, 10-dihydro-9-acridinone

phenol

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