ethyl (5-{3-[4-(2-bromo-5-fluorophenoxy)butoxy]isoxazol-5-yl}-2H-tetrazol-2-yl)acetate

Base Information

Chemical Name:ethyl (5-{3-[4-(2-bromo-5-fluorophenoxy)butoxy]isoxazol-5-yl}-2H-tetrazol-2-yl)acetate
CAS No.:1073319-30-8
Molecular Formula:C₁₈H₁₉BrFN₅O₅
Molecular Weight:484.282
Hs Code.:

Synonyms:ethyl (5-{3-[4-(2-bromo-5-fluorophenoxy)butoxy]isoxazol-5-yl}-2H-tetrazol-2-yl)acetate

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Chemical Property of ethyl (5-{3-[4-(2-bromo-5-fluorophenoxy)butoxy]isoxazol-5-yl}-2H-tetrazol-2-yl)acetate

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Technology Process of ethyl (5-{3-[4-(2-bromo-5-fluorophenoxy)butoxy]isoxazol-5-yl}-2H-tetrazol-2-yl)acetate

There total 6 articles about ethyl (5-{3-[4-(2-bromo-5-fluorophenoxy)butoxy]isoxazol-5-yl}-2H-tetrazol-2-yl)acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1073319-14-8
1-bromo-2-(4-bromobutoxy)-4-fluorobenzene

: 1073318-87-2
ethyl [5-(3-hydroxyisoxazol-5-yl)-2H-tetrazol-2-yl]acetate

: 1073319-30-8
ethyl (5-{3-[4-(2-bromo-5-fluorophenoxy)butoxy]isoxazol-5-yl}-2H-tetrazol-2-yl)acetate

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 0 - 60 ℃; for 1.5h;

Reference yield:

: 1367486-35-8
C₁₄H₁₃BrFN₅O₃

: 105-36-2
ethyl bromoacetate

: 1073319-30-8
ethyl (5-{3-[4-(2-bromo-5-fluorophenoxy)butoxy]isoxazol-5-yl}-2H-tetrazol-2-yl)acetate

: C₁₇H₁₇BrFN₅O₅

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In 1,4-dioxane; at 90 ℃; for 1h;
DOI:10.1016/j.bmcl.2011.10.070

Reference yield:

: 1073318-93-0
ethyl (5-{3-[(4-methoxybenzyl)oxy]isoxazol-5-yl}-2H-tetrazol-2-yl)acetate

: 1073319-30-8
ethyl (5-{3-[4-(2-bromo-5-fluorophenoxy)butoxy]isoxazol-5-yl}-2H-tetrazol-2-yl)acetate

Guidance literature:: Multi-step reaction with 2 steps

1: dimethylsulfide; trifluoroacetic acid / dichloromethane / 3 h / 0 - 20 °C

2: potassium carbonate / N,N-dimethyl-formamide / 1.5 h / 0 - 60 °C

With dimethylsulfide; potassium carbonate; trifluoroacetic acid; In dichloromethane; N,N-dimethyl-formamide;