3-azido-5-O-benzoyl-2,3-dideoxy-4-O-mesyl-D-erythro-pentose dimethyl acetal

Base Information

Chemical Name:3-azido-5-O-benzoyl-2,3-dideoxy-4-O-mesyl-D-erythro-pentose dimethyl acetal
CAS No.:143764-05-0
Molecular Formula:C₁₅H₂₁N₃O₇S
Molecular Weight:387.414
Hs Code.:

Synonyms:3-azido-5-O-benzoyl-2,3-dideoxy-4-O-mesyl-D-erythro-pentose dimethyl acetal

Suppliers and Price of 3-azido-5-O-benzoyl-2,3-dideoxy-4-O-mesyl-D-erythro-pentose dimethyl acetal

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-azido-5-O-benzoyl-2,3-dideoxy-4-O-mesyl-D-erythro-pentose dimethyl acetal

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Technology Process of 3-azido-5-O-benzoyl-2,3-dideoxy-4-O-mesyl-D-erythro-pentose dimethyl acetal

There total 6 articles about 3-azido-5-O-benzoyl-2,3-dideoxy-4-O-mesyl-D-erythro-pentose dimethyl acetal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 67-56-1
methanol

: 143764-04-9
3-azido-5-O-benzoyl-2,3-dideoxy-4-O-mesyl-D-erythro-pentose diisobutyl dithioacetal

: 143764-05-0
3-azido-5-O-benzoyl-2,3-dideoxy-4-O-mesyl-D-erythro-pentose dimethyl acetal

Guidance literature:: With mercury dichloride; mercury(II) oxide; at 60 ℃; for 2h;
DOI:10.1016/0008-6215(94)00296-R

Reference yield:

: 98-88-4
benzoyl chloride

: 143764-05-0
3-azido-5-O-benzoyl-2,3-dideoxy-4-O-mesyl-D-erythro-pentose dimethyl acetal

Guidance literature:: Multi-step reaction with 3 steps

1: 77 percent / pyridine / CHCl₃ / 1.) 0 deg C, 4 h, 2.) RT, 16 h

2: 90 percent / Et₃N / CH₂Cl₂ / 1.) 0 deg C, 30 min, 2.) RT, 2 h

3: 70 percent / mercuric oxide, mercuric chloride / 2 h / 60 °C

With pyridine; triethylamine; mercury dichloride; mercury(II) oxide; In dichloromethane; chloroform;
DOI:10.1016/0008-6215(94)00296-R

Reference yield:

: 2-deoxy-4,5-O-isopropylidene-D-threo-pentose diisobutyl dithioacetal

: 143764-05-0
3-azido-5-O-benzoyl-2,3-dideoxy-4-O-mesyl-D-erythro-pentose dimethyl acetal

Guidance literature:: Multi-step reaction with 5 steps

1: 75 percent / PPh₃, Zn(N₃)2*(C₅H₅N)2, diisopropyl azodicarboxylate / toluene / 3 h

2: 87 percent / Amberlite 15 (H⁺ form), water / ethanol

3: 77 percent / pyridine / CHCl₃ / 1.) 0 deg C, 4 h, 2.) RT, 16 h

4: 90 percent / Et₃N / CH₂Cl₂ / 1.) 0 deg C, 30 min, 2.) RT, 2 h

5: 70 percent / mercuric oxide, mercuric chloride / 2 h / 60 °C

With pyridine; Zn(N₃)2/bis-pyridine complex; di-isopropyl azodicarboxylate; Amberlite 15 (H⁺ form); water; triethylamine; triphenylphosphine; mercury dichloride; mercury(II) oxide; In ethanol; dichloromethane; chloroform; toluene;
DOI:10.1016/0008-6215(94)00296-R