N-Fmoc-Phe-SPh

Base Information

Chemical Name:N-Fmoc-Phe-SPh
CAS No.:1359014-85-9
Molecular Formula:C₃₀H₂₅NO₃S
Molecular Weight:479.599
Hs Code.:

Synonyms:N-Fmoc-Phe-SPh

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-Fmoc-Phe-SPh

Chemical Property:

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Technology Process of N-Fmoc-Phe-SPh

There total 1 articles about N-Fmoc-Phe-SPh which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 35661-40-6
N-Fmoc L-Phe

: 108-98-5
thiophenol

: 1359014-85-9
N-Fmoc-Phe-SPh

Guidance literature:: With dicyclohexyl-carbodiimide; In ethyl acetate; at 20 ℃; for 24h; Inert atmosphere;
DOI:10.1021/ol203399x

Reference yield: 79.0%

: 1359014-85-9
N-Fmoc-Phe-SPh

: 1359015-26-1
(9H-fluoren-9-yl)methyl styrylcarbamate

: 1359015-03-4
(9H-fluoren-9-yl)methyl styrylcarbamate

Guidance literature:: N-Fmoc-Phe-SPh; With copper(I) 2-hydroxy-3-methylbenzoate; palladium diacetate; triethyl phosphite; In 1,4-dioxane; at 50 ℃; for 1h; Inert atmosphere;

With palladium diacetate; triethyl phosphite; In 1,4-dioxane; at 50 ℃; for 2h; optical yield given as %de; Inert atmosphere;
DOI:10.1021/ol203399x

Reference yield:

: 1359014-85-9
N-Fmoc-Phe-SPh

: 2491-20-5
L-alanine methyl ester hydrochloride

: 118474-95-6
(S)-methyl 2-((S)-2-((((9H-fluoren-9-yl)methoxy)carbonyl)amino)-3-phenylpropanamido)propanoate

Guidance literature:: With 1-(3,5-bis(trifluoromethyl)phenyl)-3-(3'-mercapto-4'-((dimethylamino)methyl)-[1,1'-biphenyl]-2-yl)urea; triethylamine; In toluene; at 20 ℃;
DOI:10.1021/acs.orglett.7b02412