(9H-fluoren-9-yl)methyl styrylcarbamate

Base Information

Chemical Name:(9H-fluoren-9-yl)methyl styrylcarbamate
CAS No.:1359015-03-4
Molecular Formula:C₂₃H₁₉NO₂
Molecular Weight:341.409
Hs Code.:

Synonyms:(9H-fluoren-9-yl)methyl styrylcarbamate

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Chemical Property of (9H-fluoren-9-yl)methyl styrylcarbamate

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Technology Process of (9H-fluoren-9-yl)methyl styrylcarbamate

There total 4 articles about (9H-fluoren-9-yl)methyl styrylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 1359014-85-9
N-Fmoc-Phe-SPh

: 1359015-26-1
(9H-fluoren-9-yl)methyl styrylcarbamate

: 1359015-03-4
(9H-fluoren-9-yl)methyl styrylcarbamate

Guidance literature:: N-Fmoc-Phe-SPh; With copper(I) 2-hydroxy-3-methylbenzoate; palladium diacetate; triethyl phosphite; In 1,4-dioxane; at 50 ℃; for 1h; Inert atmosphere;

With palladium diacetate; triethyl phosphite; In 1,4-dioxane; at 50 ℃; for 2h; optical yield given as %de; Inert atmosphere;
DOI:10.1021/ol203399x

Reference yield:

: 35661-40-6
N-Fmoc L-Phe

: 1359015-26-1
(9H-fluoren-9-yl)methyl styrylcarbamate

: 1359015-03-4
(9H-fluoren-9-yl)methyl styrylcarbamate

Guidance literature:: Multi-step reaction with 2 steps

1.1: dicyclohexyl-carbodiimide / ethyl acetate / 24 h / 20 °C / Inert atmosphere

2.1: copper(I) 2-hydroxy-3-methylbenzoate; palladium diacetate; triethyl phosphite / 1,4-dioxane / 1 h / 50 °C / Inert atmosphere

2.2: 2 h / 50 °C / Inert atmosphere

With copper(I) 2-hydroxy-3-methylbenzoate; palladium diacetate; dicyclohexyl-carbodiimide; triethyl phosphite; In 1,4-dioxane; ethyl acetate;
DOI:10.1021/ol203399x

Reference yield:

: 126727-04-6
2-(9-fluorenylmethoxycarbonylamino)-3-phenylpropionic acid

: 1359015-26-1
(9H-fluoren-9-yl)methyl styrylcarbamate

: 1359015-03-4
(9H-fluoren-9-yl)methyl styrylcarbamate

Guidance literature:: Multi-step reaction with 2 steps

1: diisopropyl-carbodiimide / dichloromethane

2: sodium iodide / acetone / Irradiation

With sodium iodide; diisopropyl-carbodiimide; In dichloromethane; acetone;
DOI:10.1039/d1sc01024g