[1-[5-(4-Methoxy-benzyloxy)-2-nitro-phenyl]-meth-(Z)-ylidene]-p-tolyl-amine

Base Information

• Chemical Name: [1-[5-(4-Methoxy-benzyloxy)-2-nitro-phenyl]-meth-(Z)-ylidene]-p-tolyl-amine
• CAS No.: 77405-70-0
• Molecular Formula: C₂₂H₂₀N₂O₄
• Molecular Weight: 376.412

Synonyms:[1-[5-(4-Methoxy-benzyloxy)-2-nitro-phenyl]-meth-(Z)-ylidene]-p-tolyl-amine

Chemical Property of [1-[5-(4-Methoxy-benzyloxy)-2-nitro-phenyl]-meth-(Z)-ylidene]-p-tolyl-amine

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Technology Process of [1-[5-(4-Methoxy-benzyloxy)-2-nitro-phenyl]-meth-(Z)-ylidene]-p-tolyl-amine

There total 3 articles about [1-[5-(4-Methoxy-benzyloxy)-2-nitro-phenyl]-meth-(Z)-ylidene]-p-tolyl-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-nitro-5-hydroxybenzaldehyde (42454-06-8) → [1-[5-(4-Methoxy-benzyloxy)-2-nitro-phenyl]-meth-(Z)-ylidene]-p-tolyl-amine (77405-70-0)

Guidance literature:

Multi-step reaction with 2 steps

1: K₂CO₃, KI / dimethylformamide / 14 h / Ambient temperature

2: benzene / 14 h / Heating

With potassium carbonate; potassium iodide; In N,N-dimethyl-formamide; benzene;

DOI:10.1021/ja00395a071

Reference yield:

p-Methoxybenzyl bromide (2746-25-0) → [1-[5-(4-Methoxy-benzyloxy)-2-nitro-phenyl]-meth-(Z)-ylidene]-p-tolyl-amine (77405-70-0)

Guidance literature:

Multi-step reaction with 2 steps

1: K₂CO₃, KI / dimethylformamide / 14 h / Ambient temperature

2: benzene / 14 h / Heating

With potassium carbonate; potassium iodide; In N,N-dimethyl-formamide; benzene;

DOI:10.1021/ja00395a071

Reference yield:

p-toluidine (106-49-0,12221-03-3) + 5-(4-methoxybenzyloxy)-2-nitrobenzaldehyde (77405-69-7) → [1-[5-(4-Methoxy-benzyloxy)-2-nitro-phenyl]-meth-(Z)-ylidene]-p-tolyl-amine (77405-70-0)

Guidance literature:

In benzene; for 14h; Heating;

DOI:10.1021/ja00395a071

upstream raw materials:

p-toluidine

5-(4-methoxybenzyloxy)-2-nitrobenzaldehyde

2-nitro-5-hydroxybenzaldehyde

p-Methoxybenzyl bromide

Downstream raw materials:

methyl 5-amino-4-<2-(benzyloxy)-3,4-dimethoxyphenyl>-6-(6-methoxy-5-nitro-2-quinolyl)-3-methylpyridine-2-carboxylate

2-[4-(2-Benzyloxy-3,4-dimethoxy-phenyl)-5,6-dimethyl-3-vinyl-pyridin-2-yl]-quinolin-6-ol

2-[4-(2-Benzyloxy-3,4-dimethoxy-phenyl)-5,6-dimethyl-3-vinyl-pyridin-2-yl]-6-methoxy-5-nitro-quinoline

5-Amino-6-(5-amino-6-methoxy-quinolin-2-yl)-4-(2-benzyloxy-3,4-dimethoxy-phenyl)-3-methyl-pyridine-2-carboxylic acid methyl ester

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