N⁴--N¹,N⁷-bis(2,3-dimethoxybenzoyl)bis(3-aminopropyl)amine

Base Information

Chemical Name:N⁴--N¹,N⁷-bis(2,3-dimethoxybenzoyl)bis(3-aminopropyl)amine
CAS No.:78217-79-5
Molecular Formula:C₃₃H₄₀N₄O₉
Molecular Weight:636.702
Hs Code.:

N<sup>4</sup>-<N-(2-hydroxybenzoyl)glycyl>-N<sup>1</sup>,N<sup>7</sup>-bis(2,3-dimethoxybenzoyl)bis(3-aminopropyl)amine

Synonyms:N⁴--N¹,N⁷-bis(2,3-dimethoxybenzoyl)bis(3-aminopropyl)amine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N⁴--N¹,N⁷-bis(2,3-dimethoxybenzoyl)bis(3-aminopropyl)amine

Chemical Property:

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Technology Process of N⁴--N¹,N⁷-bis(2,3-dimethoxybenzoyl)bis(3-aminopropyl)amine

There total 5 articles about N⁴--N¹,N⁷-bis(2,3-dimethoxybenzoyl)bis(3-aminopropyl)amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 2-(2-trifluoroacetoxyphenyl)-5-oxazolone

: 78217-76-2
N¹,N⁷-bis(2,3-dimethoxybenzoyl)bis(3-aminopropyl)amine

: 78217-79-5
N⁴--N¹,N⁷-bis(2,3-dimethoxybenzoyl)bis(3-aminopropyl)amine

Guidance literature:: With triethylamine; In dichloromethane; for 40h; -78 deg C to room temperature;
DOI:10.1021/jo00335a041

Reference yield:

: 782-87-6
N-benzylbis(2-cyanoethyl)amine

: 78217-79-5
N⁴--N¹,N⁷-bis(2,3-dimethoxybenzoyl)bis(3-aminopropyl)amine

Guidance literature:: Multi-step reaction with 4 steps

1: 67 percent / LiAlH₄, AlCl₃

2: 97 percent / triethylamine / CH₂Cl₂ / 0 deg C to room temperature

3: 98 percent / 1) H₂, 2) NaOMe / 1) PdCl₂ / 1) glacial acetic acid, room temperature, 2) MeOH, 30 min

4: 93 percent / triethylamine / CH₂Cl₂ / 40 h / -78 deg C to room temperature

With lithium aluminium tetrahydride; aluminium trichloride; hydrogen; sodium methylate; triethylamine; palladium dichloride; In dichloromethane;
DOI:10.1021/jo00335a041

Reference yield:

: 1555-71-1
N1-(3-amino-propyl)-N1-benzyl-propane-1,3-diamine

: 78217-79-5
N⁴--N¹,N⁷-bis(2,3-dimethoxybenzoyl)bis(3-aminopropyl)amine

Guidance literature:: Multi-step reaction with 3 steps

1: 97 percent / triethylamine / CH₂Cl₂ / 0 deg C to room temperature

2: 98 percent / 1) H₂, 2) NaOMe / 1) PdCl₂ / 1) glacial acetic acid, room temperature, 2) MeOH, 30 min

3: 93 percent / triethylamine / CH₂Cl₂ / 40 h / -78 deg C to room temperature

With hydrogen; sodium methylate; triethylamine; palladium dichloride; In dichloromethane;
DOI:10.1021/jo00335a041