4-n-hexyl-4'-(3-bromo)propyloxyazobenzene

Base Information

• Chemical Name: 4-n-hexyl-4'-(3-bromo)propyloxyazobenzene
• CAS No.: 215095-95-7
• Molecular Formula: C₂₁H₂₇BrN₂O
• Molecular Weight: 403.362
• Mol file: 215095-95-7.mol

Synonyms:4-n-hexyl-4'-(3-bromo)propyloxyazobenzene

Chemical Property of 4-n-hexyl-4'-(3-bromo)propyloxyazobenzene

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 4-n-hexyl-4'-(3-bromo)propyloxyazobenzene

There total 3 articles about 4-n-hexyl-4'-(3-bromo)propyloxyazobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

4-(4-n-hexyl-phenylazo)phenol (104648-88-6,33228-49-8) + 1,3-dibromo-propane (109-64-8) → 4-n-hexyl-4'-(3-bromo)propyloxyazobenzene (215095-95-7)

Guidance literature:

With potassium carbonate; In acetone; for 20h; Inert atmosphere; Reflux;

DOI:10.1246/cl.2010.1144

Reference yield:

4-hexylaniline (33228-45-4) → 4-n-hexyl-4'-(3-bromo)propyloxyazobenzene (215095-95-7)

Guidance literature:

Multi-step reaction with 2 steps

1: conc. HCl, NaNO₂, Na₂CO₃

2: KOH / tetrahydrofuran

With hydrogenchloride; potassium hydroxide; sodium carbonate; sodium nitrite; In tetrahydrofuran;

DOI:10.1080/00397919808004930

Reference yield:

phenol (108-95-2,27073-41-2) → 4-n-hexyl-4'-(3-bromo)propyloxyazobenzene (215095-95-7)

Guidance literature:

Multi-step reaction with 2 steps

1: conc. HCl, NaNO₂, Na₂CO₃

2: KOH / tetrahydrofuran

With hydrogenchloride; potassium hydroxide; sodium carbonate; sodium nitrite; In tetrahydrofuran;

DOI:10.1080/00397919808004930

upstream raw materials:

4-(4-n-hexyl-phenylazo)phenol

1,3-dibromo-propane

4-hexylaniline

phenol