(S)-2-((R)-2-Benzyloxy-1-hydroxy-ethyl)-5-methyl-hex-4-enoic acid methoxy-methyl-amide

Base Information

• Chemical Name: (S)-2-((R)-2-Benzyloxy-1-hydroxy-ethyl)-5-methyl-hex-4-enoic acid methoxy-methyl-amide
• CAS No.: 733000-61-8
• Molecular Formula: C₁₈H₂₇NO₄
• Molecular Weight: 321.417

Synonyms:(S)-2-((R)-2-Benzyloxy-1-hydroxy-ethyl)-5-methyl-hex-4-enoic acid methoxy-methyl-amide

Chemical Property of (S)-2-((R)-2-Benzyloxy-1-hydroxy-ethyl)-5-methyl-hex-4-enoic acid methoxy-methyl-amide

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Technology Process of (S)-2-((R)-2-Benzyloxy-1-hydroxy-ethyl)-5-methyl-hex-4-enoic acid methoxy-methyl-amide

There total 1 articles about (S)-2-((R)-2-Benzyloxy-1-hydroxy-ethyl)-5-methyl-hex-4-enoic acid methoxy-methyl-amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

N,O-dimethylhydroxylamine*hydrochloride (6638-79-5) + (S)-2-((R)-2-Benzyloxy-1-hydroxy-ethyl)-5-methyl-hex-4-enoic acid ethyl ester (733000-60-7) → (S)-2-((R)-2-Benzyloxy-1-hydroxy-ethyl)-5-methyl-hex-4-enoic acid methoxy-methyl-amide (733000-61-8)

Guidance literature:

With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 2h;

DOI:10.1002/ejoc.200400047

Reference yield: 98.0%

t-butyldimethylsiyl triflate (69739-34-0) + (S)-2-((R)-2-Benzyloxy-1-hydroxy-ethyl)-5-methyl-hex-4-enoic acid methoxy-methyl-amide (733000-61-8) → (S)-2-[(R)-2-Benzyloxy-1-(tert-butyl-dimethyl-silanyloxy)-ethyl]-5-methyl-hex-4-enoic acid methoxy-methyl-amide (733000-64-1)

Guidance literature:

With 2,6-dimethylpyridine; In dichloromethane; at 0 ℃; for 1h;

DOI:10.1002/ejoc.200400047

Reference yield: 63.0%

octyllithium (3314-49-6) + (S)-2-((R)-2-Benzyloxy-1-hydroxy-ethyl)-5-methyl-hex-4-enoic acid methoxy-methyl-amide (733000-61-8) → (S)-2-((R)-2-Benzyloxy-1-hydroxy-ethyl)-5-methyl-hex-4-enoic acid methylamide

Guidance literature:

In tetrahydrofuran; at -40 ℃; for 3h;

DOI:10.1002/ejoc.200400047

upstream raw materials:

N,O-dimethylhydroxylamine*hydrochloride

(S)-2-((R)-2-Benzyloxy-1-hydroxy-ethyl)-5-methyl-hex-4-enoic acid ethyl ester

Downstream raw materials:

(S)-2-[(R)-2-Benzyloxy-1-(tert-butyl-dimethyl-silanyloxy)-ethyl]-5-methyl-hex-4-enoic acid methoxy-methyl-amide

(S)-5-((R)-2-Benzyloxy-1-hydroxy-ethyl)-2-methyl-tetradec-2-en-6-one

(S)-5-[(R)-2-Benzyloxy-1-(tert-butyl-dimethyl-silanyloxy)-ethyl]-2-methyl-tetradec-2-en-6-one

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