N-[4-benzyloxy-2-(1-hydroxybut-3-enyl)phenyl]-4-methylbenzenesulfonamide

Base Information

Chemical Name:N-[4-benzyloxy-2-(1-hydroxybut-3-enyl)phenyl]-4-methylbenzenesulfonamide
CAS No.:791810-63-4
Molecular Formula:C₂₄H₂₅NO₄S
Molecular Weight:423.533
Hs Code.:

Synonyms:N-[4-benzyloxy-2-(1-hydroxybut-3-enyl)phenyl]-4-methylbenzenesulfonamide

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Chemical Property of N-[4-benzyloxy-2-(1-hydroxybut-3-enyl)phenyl]-4-methylbenzenesulfonamide

Chemical Property:

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Technology Process of N-[4-benzyloxy-2-(1-hydroxybut-3-enyl)phenyl]-4-methylbenzenesulfonamide

There total 4 articles about N-[4-benzyloxy-2-(1-hydroxybut-3-enyl)phenyl]-4-methylbenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1730-25-2
allylmagnesium bromide

: 760968-80-7
N-(4-benzyloxy-2-formylphenyl)-4-methylbenzenesulfonamide

: 791810-63-4
N-[4-benzyloxy-2-(1-hydroxybut-3-enyl)phenyl]-4-methylbenzenesulfonamide

Guidance literature:: In tetrahydrofuran; diethyl ether; at -10 ℃; for 2h;
DOI:10.1016/j.tet.2004.08.014

Reference yield:

: 1882-72-0
methyl 2-amino-5-hydroxybenzoate

: 791810-63-4
N-[4-benzyloxy-2-(1-hydroxybut-3-enyl)phenyl]-4-methylbenzenesulfonamide

Guidance literature:: Multi-step reaction with 5 steps

1: pyridine / 5 h / 20 °C

2: 93.3 percent / NaH / dimethylformamide / 15 h / 0 °C

3: 100 percent / LiBH₄ / tetrahydrofuran / 20 h / Heating

4: 80 percent / pyridinium dichromate / CH₂Cl₂ / 3 h / 20 °C

5: 100 percent / diethyl ether; tetrahydrofuran / 2 h / -10 °C

With pyridine; dipyridinium dichromate; lithium borohydride; sodium hydride; In tetrahydrofuran; diethyl ether; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.tet.2004.08.014

Reference yield:

: 760968-79-4
N-(4-benzyloxy-2-hydroxymethylphenyl)-4-methylbenzenesulfonamide

: 791810-63-4
N-[4-benzyloxy-2-(1-hydroxybut-3-enyl)phenyl]-4-methylbenzenesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / pyridinium dichromate / CH₂Cl₂ / 3 h / 20 °C

2: 100 percent / diethyl ether; tetrahydrofuran / 2 h / -10 °C

With dipyridinium dichromate; In tetrahydrofuran; diethyl ether; dichloromethane;
DOI:10.1016/j.tet.2004.08.014