(R)-2-Hydroxy-1-((1S,4R,7R)-7-methylsulfanyl-2-oxa-3-aza-bicyclo[2.2.1]hept-5-en-3-yl)-2-phenyl-ethanone

Base Information

Chemical Name:(R)-2-Hydroxy-1-((1S,4R,7R)-7-methylsulfanyl-2-oxa-3-aza-bicyclo[2.2.1]hept-5-en-3-yl)-2-phenyl-ethanone
CAS No.:134153-71-2
Molecular Formula:C₁₄H₁₅NO₃S
Molecular Weight:277.344
Hs Code.:

Synonyms:(R)-2-Hydroxy-1-((1S,4R,7R)-7-methylsulfanyl-2-oxa-3-aza-bicyclo[2.2.1]hept-5-en-3-yl)-2-phenyl-ethanone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (R)-2-Hydroxy-1-((1S,4R,7R)-7-methylsulfanyl-2-oxa-3-aza-bicyclo[2.2.1]hept-5-en-3-yl)-2-phenyl-ethanone

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Technology Process of (R)-2-Hydroxy-1-((1S,4R,7R)-7-methylsulfanyl-2-oxa-3-aza-bicyclo[2.2.1]hept-5-en-3-yl)-2-phenyl-ethanone

There total 4 articles about (R)-2-Hydroxy-1-((1S,4R,7R)-7-methylsulfanyl-2-oxa-3-aza-bicyclo[2.2.1]hept-5-en-3-yl)-2-phenyl-ethanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 2.0%

: 124412-11-9
1-(methylthio)cyclopenta-2,4-diene

: 127649-02-9
(R)-(-)-mandelohydroxamic acid

: 134153-71-2
(1R,4S,7R)-3-(2-(R)-hydroxy-2-phenylacetyl)-7-(methylthio)-2-oxa-3-azabicyclo<2.2.1>hept-5-ene

: (1S,4R,7S)-3-(2-(R)-hydroxy-2-phenylacetyl)-7-(methylthio)-2-oxa-3-azabicyclo<2.2.1>hept-5-ene

Guidance literature:: With tetrabutylammonium periodite; In methanol; tetrachloromethane; at 0 ℃; for 1h;
DOI:10.1021/ja00081a017

Reference yield:

: 124412-11-9
1-(methylthio)cyclopenta-2,4-diene

: 126924-19-4
(2R)-(-)-2-hydroxy-2-phenylacetohydroxamic acid

: 134153-71-2
(R)-2-Hydroxy-1-((1S,4R,7R)-7-methylsulfanyl-2-oxa-3-aza-bicyclo[2.2.1]hept-5-en-3-yl)-2-phenyl-ethanone

: 134153-71-2
(1R,4S,7R)-3-(2-(R)-hydroxy-2-phenylacetyl)-7-(methylthio)-2-oxa-3-azabicyclo<2.2.1>hept-5-ene

Guidance literature:: With tetrabutylammonium periodite; In methanol; at 0 ℃; for 1h; Yield given. Yields of byproduct given;
DOI:10.1021/ja00013a071

Reference yield:

: 124412-11-9
1-(methylthio)cyclopenta-2,4-diene

: 126924-19-4
(2R)-(-)-2-hydroxy-2-phenylacetohydroxamic acid

: 134153-71-2
(R)-2-Hydroxy-1-((1S,4R,7R)-7-methylsulfanyl-2-oxa-3-aza-bicyclo[2.2.1]hept-5-en-3-yl)-2-phenyl-ethanone

: 134153-71-2
(1R,4S,7R)-3-(2-(R)-hydroxy-2-phenylacetyl)-7-(methylthio)-2-oxa-3-azabicyclo<2.2.1>hept-5-ene

Guidance literature:: With tetrabutylammonium periodite; In methanol; at 0 ℃; for 1h; Yield given. Yields of byproduct given;
DOI:10.1021/ja00013a071