O--3-nitro-acetophenonoxim

Base Information

• Chemical Name: O--3-nitro-acetophenonoxim
• CAS No.: 3065-01-8
• Molecular Formula: C₁₈H₁₇N₃O₆
• Molecular Weight: 371.349

Synonyms:O--3-nitro-acetophenonoxim

Chemical Property of O--3-nitro-acetophenonoxim

Chemical Property:

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Technology Process of O--3-nitro-acetophenonoxim

There total 2 articles about O--3-nitro-acetophenonoxim which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.4%

(E)-1-(3-nitrophenyl)ethan-1-one oxime (87974-55-8) + N-(Benzyloxycarbonyl)glycine (1138-80-3) → O--3-nitro-acetophenonoxim (3065-01-8)

Guidance literature:

With dicyclohexyl-carbodiimide; In N,N-dimethyl-formamide;

DOI:10.1246/bcsj.56.2432

Reference yield:

m-nitroacetophenone oxime (7471-32-1) + N-(Benzyloxycarbonyl)glycine (1138-80-3) → O--3-nitro-acetophenonoxim (3065-01-8)

Guidance literature:

Multistep reaction; (i) ClCO₂Et, Et₃N, (ii) /BRN= 2211982/;

upstream raw materials:

(E)-1-(3-nitrophenyl)ethan-1-one oxime

N-(Benzyloxycarbonyl)glycine

m-nitroacetophenone oxime

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