N- (3-formic acid methyl phenyl)sydnone

Base Information

Chemical Name:N- (3-formic acid methyl phenyl)sydnone
CAS No.:841260-62-6
Molecular Formula:C₁₀H₈N₂O₄
Molecular Weight:220.185
Hs Code.:

Synonyms:N- (3-formic acid methyl phenyl)sydnone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N- (3-formic acid methyl phenyl)sydnone

Chemical Property:

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Technology Process of N- (3-formic acid methyl phenyl)sydnone

There total 3 articles about N- (3-formic acid methyl phenyl)sydnone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 67-56-1
methanol

: 841260-55-7
3-(3-carboxyphenyl)sydnone

: 841260-62-6
N- (3-formic acid methyl phenyl)sydnone

Guidance literature:: With sulfuric acid; at 20 ℃; for 24h;
DOI:10.1002/ardp.200300847

Reference yield:

: 81189-31-3
N-(3-carboxyphenyl)glycine

: 841260-62-6
N- (3-formic acid methyl phenyl)sydnone

Guidance literature:: Multi-step reaction with 3 steps

1: 73 percent / hydrochloric acid; sodium nitrite / H₂O / 1.5 h / 0 - 5 °C

2: 80 percent / acetic anhydride / 3 h / Heating

3: 80 percent / conc. H₂SO₄ / 24 h / 20 °C

With hydrogenchloride; sulfuric acid; acetic anhydride; sodium nitrite; In water;
DOI:10.1002/ardp.200300847

Reference yield:

: 841260-54-6
N-nitroso-N-(3-carboxyphenyl)glycine

: 841260-62-6
N- (3-formic acid methyl phenyl)sydnone

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / acetic anhydride / 3 h / Heating

2: 80 percent / conc. H₂SO₄ / 24 h / 20 °C

With sulfuric acid; acetic anhydride;
DOI:10.1002/ardp.200300847